1-(苯基甲基)萘-2-醇合成路线 （共 37 条）
反应条件
1: 72 percent / p-toluenesulfonic acid / 0.02 h / microwave irradiation 2: 59.3 percent / HCO2NH4 / Pd/C / methanol / 2 h / Heating View Scheme
参考文献
Katritzky, Alan R.; Lan, Xiangfu; Lam, Jamshed N.
Chemische Berichte, 1991 , vol. 124, # 8 p. 1809 - 1817
反应条件
1: 79.7 percent / p-toluenesulfonic acid / 0.02 h / microwave irradiation 2: 82 percent / HCO2NH4 / Pd/C / methanol / 2 h / Heating View Scheme
参考文献
Paul, Nawal K.; Dietrich, Lindsay; Jha, Amitabh
Synthetic Communications, 2007 , vol. 37, # 6 p. 877 - 888
反应条件
1: 72 percent / p-toluenesulfonic acid / 0.02 h / microwave irradiation 2: 59.3 percent / HCO2NH4 / Pd/C / methanol / 2 h / Heating View Scheme
参考文献
Paul, Nawal K.; Dietrich, Lindsay; Jha, Amitabh
Synthetic Communications, 2007 , vol. 37, # 6 p. 877 - 888
反应条件
1: 68 percent / toluene / Heating 2: 52 percent / Sodium sulfide (hydrated) / ethanol / 12 h / Heating 3: 94 percent / LiAlH4 / diethyl ether / 12 h / Heating 4: 40 percent / NaI, trimethylsilyl chloride / acetonitrile / 1 h / 22 °C View Scheme
参考文献
Smith, James G.; Welankiwar, Sudha S.; Shantz, Barry S.; Lai, Eric H.; Chu, Noreen G.
Journal of Organic Chemistry, 1980 , vol. 45, # 10 p. 1817 - 1824
反应条件
1: 52 percent / Sodium sulfide (hydrated) / ethanol / 12 h / Heating 2: 94 percent / LiAlH4 / diethyl ether / 12 h / Heating 3: 40 percent / NaI, trimethylsilyl chloride / acetonitrile / 1 h / 22 °C View Scheme
参考文献
Smith, James G.; Welankiwar, Sudha S.; Shantz, Barry S.; Lai, Eric H.; Chu, Noreen G.
Journal of Organic Chemistry, 1980 , vol. 45, # 10 p. 1817 - 1824
反应条件
1: 94 percent / LiAlH4 / diethyl ether / 12 h / Heating 2: 40 percent / NaI, trimethylsilyl chloride / acetonitrile / 1 h / 22 °C View Scheme
参考文献
Smith, James G.; Welankiwar, Sudha S.; Shantz, Barry S.; Lai, Eric H.; Chu, Noreen G.
Journal of Organic Chemistry, 1980 , vol. 45, # 10 p. 1817 - 1824
反应条件
sodium hydroxide; polystyrene bonded phosphonium salts in toluene T=55°C; 18 h; C/O-alkylation ratio; phase-transfer conditions or EtOH-H2O (1.5:1 v/v) as solvent; Dowex-1, SiO2-bonded phosphonium salt or without catalyst; KineticsProduct distributionRate constant;
参考文献
Montanari, Fernando; Quici, Silvio; Tundo, Pietro
Journal of Organic Chemistry, 1983 , vol. 48, # 2 p. 199 - 202
反应条件
methanol; sodium methylate T=220°C;
参考文献
Cornforth; Cornforth; Robinson
Journal of the Chemical Society, 1942 , p. 682,684
Journal of the Chemical Society, 1943 , p. 168
反应条件
1: 38 percent / piperidine / toluene / 24 h / Heating 2: 90 percent / LiAlH4 / tetrahydrofuran / 22 h / Heating View Scheme
参考文献
Katritzky, Alan R.; Lan, Xiangfu; Lam, Jamshed N.
Chemische Berichte, 1991 , vol. 124, # 8 p. 1809 - 1817
反应条件
aluminum oxide; sodium methylate T=50°C; 48 h; Yield given. Yields of byproduct given;
参考文献
Bram, Georges; Geraghty, Niall; Nee, Gerard; Seyden-Penne, Jacqueline
Journal of the Chemical Society, Chemical Communications, 1980 , # 7 p. 325 - 326
