3-氰基-1,2,4-三氮唑合成路线 （共 4 条）
反应条件
hydrogenchloride in 1,4-dioxane T=0 - 20°C; Inert atmosphere;
参考文献
Ampac Fine Chemicals LLC
Patent: US2009/292122 A1, 2009 ;
Location in patent: Page/Page column 11 ;
反应条件
trifluoroacetic anhydride in 1,4-dioxane; pyridine T=-1.3 - 25°C; 72 h; Inert atmosphere; Product distribution / selectivity;
参考文献
Ampac Fine Chemicals LLC
Patent: US2009/292122 A1, 2009 ;
Location in patent: Page/Page column 12 ;
反应条件
in N,N-dimethyl-formamide 16 h; Inert atmosphereReflux;
参考文献
Ampac Fine Chemicals LLC
Patent: US2009/292122 A1, 2009 ;
Location in patent: Page/Page column 11 ;
反应条件
purine nucleoside phosphorylase from Escherichia coli in aq. phosphate buffer T=55°C; pH=7; 96 h; Enzymatic reaction;
参考文献
Konstantinova; Chudinov; Fateev; Matveev; Zhurilo; Shvets; Miroshnikov
Russian Journal of Bioorganic Chemistry, 2013 , vol. 39, # 1 p. 53 - 71
Bioorganicheskaya Khimiya, 2013 , vol. 39, # 1 p. 61 - 80,20
