反应条件
1: triethylamine; acetic acid / dichloromethane / 15 - 20 °C / pH 6-7 / |Molecular sieve
2: sodium tris(acetoxy)borohydride / dichloromethane / 16 h / 15 - 20 °C / |Molecular sieve
3: triethylamine / dichloromethane / 16 h / 15 - 20 °C / |Inert atmosphere
4: triethylamine; 1,3-bis-(diphenylphosphino)propane; palladium diacetate / 16 h / 15 - 100 °C / 3878.71 Torr
5: sodium ethanolate / ethanol / 3 h / 0 - 25 °C
View Scheme
参考文献
Lin, Jinguan; Houpis, Ioannis N.; Liu, Renmao; Wang, Youchu; Zhang, Jianqian
Organic Process Research and Development, 2014 , vol. 18, # 1 p. 205 - 214
