2,6-二硝基-4-氟苯酚合成路线 (共 9 条)
反应条件
trichloroisocyanuric acid; silica gel; sodium nitrite T=20°C; 0.25 h;
参考文献
Zolfigol, Mohammad Ali; Madrakian, Elaheh; Ghaemi, Ezat
Synlett, 2003 , # 14 p. 2222 - 2224
反应条件
TNM in acetonitrile T=25°C; Irradiation; Title compound not separated from byproducts;
参考文献
Journal of the American Chemical Society, , vol. 109, p. 7824
反应条件
cesium fluoroxysulphate in acetonitrile T=20°C; 1 h;
参考文献
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), , vol. 40, # 7.2 p. 1432 - 1436
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, , # 7 p. 1615 - 1619
反应条件
nitric acid; trifluoroacetic anhydride in acetic anhydride T=-60 - -40°C; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Tetrahedron, , vol. 45, # 5 p. 1299 - 1310
反应条件
sulfuric acid; nitric acid
参考文献
Chemische Berichte, , vol. 66, p. 1180,1183
反应条件
sulfuric acid; nitric acid Behandeln des Reaktionsproduktes mit Kalilauge;
参考文献
Chem. Zentralbl., , vol. 84, # II p. 760
参考文献
Canadian Journal of Chemistry, , vol. 67, p. 1472 - 1479
参考文献
Chemische Berichte, , vol. 66, p. 1180,1183
反应条件
thionyl chloride; N,N-dimethyl-formamide in benzene
T=20°C; 1.58333 h; Heating / reflux;
参考文献
Svenstrup, Niels; Zimmermann, Holger; Karthaus, Dagmar; Goeller, Andreas; Heimbach, Dirk; Henninger, Kerstin; Lang, Dieter; Paulsen, Daniela; Riedl, Bernd; Schohe-Loop, Rudolf; Schuhmacher, Joachim; Wunberg, Tobias
Patent: US2009/176842 A1, 2009 ;
Location in patent: Page/Page column 11-12 ;