2,4-二氟-6-硝基苯胺合成路线 (共 14 条)
参考文献
Collins Cafiero, Pamela A.; French, Colin S.; McFarlane, Michael D.; Mackie, Raymond K.; Smith, David M.
Journal of the Chemical Society - Perkin Transactions 1, 1997 , # 9 p. 1375 - 1384
反应条件
nitric acid in acetic acid T=90°C; 4 h;
参考文献
Leyva, Socorro; Castanedo, Victor; Leyva, Elisa
Journal of Fluorine Chemistry, 2003 , vol. 121, # 2 p. 171 - 175
反应条件
1: aq. HCl / 90 °C 2: 14 percent / HNO3 / acetic acid / 4 h / 90 °C View Scheme
参考文献
Journal of Fluorine Chemistry, , vol. 121, # 2 p. 171 - 175
反应条件
1: sulfuric acid; aqueous phosphoric acid; nitrosylsulfuric acid / anschliessendes Behandeln mit Natriumhypophosphit-Loesung und Kupfer(I)-oxid 2: iron; aqueous NH4Cl 4: sulfuryl chloride; disulfur dichloride; aluminium chloride View Scheme
参考文献
Finger et al.
Journal of the American Chemical Society, 1951 , vol. 73, p. 153
Journal of the American Chemical Society, 1959 , vol. 81, p. 94,98
反应条件
1: sulfuric acid; aqueous phosphoric acid; nitrosylsulfuric acid / anschliessendes Behandeln mit Natriumhypophosphit-Loesung und Kupfer(I)-oxid 2: iron; aqueous NH4Cl View Scheme
参考文献
Finger et al.
Journal of the American Chemical Society, 1951 , vol. 73, p. 153
Journal of the American Chemical Society, 1959 , vol. 81, p. 94,98
反应条件
1: sulfuric acid; aqueous phosphoric acid; nitrosylsulfuric acid / anschliessendes Behandeln mit Natriumhypophosphit-Loesung und Kupfer(I)-oxid 2: iron; aqueous NH4Cl 4: sulfuric acid; concentrated aqueous nitric acid View Scheme
参考文献
Finger et al.
Journal of the American Chemical Society, 1951 , vol. 73, p. 153
Journal of the American Chemical Society, 1959 , vol. 81, p. 94,98
反应条件
1: sulfuric acid; aqueous phosphoric acid; nitrosylsulfuric acid / anschliessendes Behandeln mit Natriumhypophosphit-Loesung und Kupfer(I)-oxid 2: iron; aqueous NH4Cl View Scheme
参考文献
Finger et al.
Journal of the American Chemical Society, 1951 , vol. 73, p. 153
Journal of the American Chemical Society, 1959 , vol. 81, p. 94,98
反应条件
hydrogen; palladium on activated charcoal in ethanol
参考文献
Dener, Jeffrey M.; O'Bryan, Colin; Yee, Robert; Shelton, Emma J.; Sperandio, David; Mahajan, Tania; Palmer, James T.; Spencer, Jeffrey R.; Tong, Zhiwei
Tetrahedron Letters, 2006 , vol. 47, # 27 p. 4591 - 4595
反应条件
1: sulfuric acid; aqueous phosphoric acid; nitrosylsulfuric acid / anschliessendes Behandeln mit Natriumhypophosphit-Loesung und Kupfer(I)-oxid 2: iron; aqueous NH4Cl 4: sulfuryl chloride; disulfur dichloride; aluminium chloride View Scheme
参考文献
Finger et al.
Journal of the American Chemical Society, 1951 , vol. 73, p. 153
Journal of the American Chemical Society, 1959 , vol. 81, p. 94,98
反应条件
1: sulfuric acid; aqueous phosphoric acid; nitrosylsulfuric acid / anschliessendes Behandeln mit Natriumhypophosphit-Loesung und Kupfer(I)-oxid 2: iron; aqueous NH4Cl 4: iron; bromine View Scheme
参考文献
Finger et al.
Journal of the American Chemical Society, 1951 , vol. 73, p. 153
Journal of the American Chemical Society, 1959 , vol. 81, p. 94,98