4-(4-甲基苯基)苯甲醛合成路线 （共 31 条）
反应条件
C25H29N3; potassium carbonate; palladium dichloride in water; N,N-dimethyl-formamide T=110°C; Suzuki-Miyaura Coupling; 8 h;
参考文献
Cao, Gao; Yang, Hai-Qing; Luo, Bao-Tian; Liu, Feng-Shou
Journal of Organometallic Chemistry, 2013 , vol. 745-746, p. 158 - 165
反应条件
Pd black; potassium carbonate in methanol; acetonitrile T=20°C; Suzuki Coupling; 2 h;
参考文献
Mandali, Pavan Kumar; Chand, Dillip Kumar
Catalysis Communications, 2013 , vol. 31, p. 16 - 20
反应条件
potassium phosphate; PdCl2(GLCAphos)2/2GLCAphos T=80°C; Substitution; 16 h;
参考文献
Karimi, Babak; Elhamifar, Dawood; Clark, James H.; Hunt, Andrew J.
Chemistry - A European Journal, 2010 , vol. 16, # 27 p. 8047 - 8053
反应条件
C22H25ClNPPdS; potassium carbonate in 1,4-dioxane T=100°C; 20 h; Inert atmosphereSchlenk technique; Overall yield = 148 mg;
参考文献
Tetrahedron Letters, , vol. 55, # 18 p. 2953 - 2956
反应条件
potassium carbonate in ethanol; water T=50°C; Suzuki-Miyaura Coupling; 19 h; Reagent/catalyst;
参考文献
Pavia, Cinzia; Ballerini, Eleonora; Bivona, Lucia Anna; Giacalone, Francesco; Aprile, Carmela; Vaccaro, Luigi; Gruttadauria, Michelangelo
Advanced Synthesis and Catalysis, 2013 , vol. 355, # 10 p. 2007 - 2018
反应条件
tetrabutyl ammonium fluoride; tetrakis(triphenylphosphine) palladium(0) in tetrahydrofuran T=50°C; 4 h;
参考文献
Hatanaka, Yasuo; Hiyama, Tamejiro
Tetrahedron Letters, 1990 , vol. 31, # 19 p. 2719 - 2722
反应条件
1: With N-bromosuccinmide in tetrachloromethane 24 h; Heating / reflux; 2: With 1,3,5,7-tetra-azatricyclo[5.1.1.13,5]decane in chloroform 5 h; Heating / reflux; 3: With hydrogenchloride; water; acetic acid more than 3 stages;
参考文献
Park, Sooyoung; Kwon, Soonki; An, Byeongkwan
Patent: US2007/149799 A1, 2007 ;
Location in patent: Page/Page column 2-3 ;
反应条件
NiCl2[(4-MeOPh)3P]2; K3PO4*3H2O; tris(4-methoxyphenyl)-phosphine in toluene T=110°C; 8 h; Inert atmosphere;
参考文献
Chen, Xiaofeng; Ke, Haihua; Zou, Gang
ACS Catalysis, 2014 , vol. 4, # 2 p. 379 - 385
反应条件
1: With sodium bis(2-methoxyethoxy)aluminium dihydride in toluene T=-15 - -5°C; 2 h; Inert atmosphereLarge scale; 2: With sulfuric acid; water in ethyl acetate; toluene T=-5 - 50°C; Inert atmosphereLarge scale; Temperature;
参考文献
Ikemoto, Tomomi; Ito, Tatsuya; Hashimoto, Hideo; Kawarasaki, Tadao; Nishiguchi, Atsuko; Mitsudera, Hiroyuki; Wakimasu, Mitsuhiro; Tomimatsu, Kiminori
Organic Process Research and Development, 2000 , vol. 4, # 6 p. 520 - 525
反应条件
dicyclohexyl(2′,6′-dimethoxybiphenyl-2-yl)phosphine; palladium diacetate; potassium carbonate in neat (no solvent) T=110°C; Suzuki-Miyaura Coupling; 24 h; Schlenk techniqueInert atmosphere;
参考文献
Asachenko, Andrey F.; Sorochkina, Kristina R.; Dzhevakov, Pavel B.; Topchiy, Maxim A.; Nechaev, Mikhail S.
Advanced Synthesis and Catalysis, 2013 , vol. 355, # 18 p. 3553 - 3557
