4,4,5,5,5-五氟戊酸合成路线 （共 4 条）
反应条件
Jone's reagent in acetone T=0 - 20°C; 1 h;
参考文献
US6645951 B1, ;
Page/Page column 281 ;
反应条件
potassium permanganate in water T=65 - 70°C;
参考文献
Organic Process Research and Development, , vol. 3, # 5 p. 363 - 364
反应条件
1: 92 percent / aq. NaOH / 1 h / Heating 2: 63 percent / CrO3, aq. AcOH / 26 h / 0 - 20 °C View Scheme
参考文献
Acta Chemica Scandinavica, , vol. 47, # 4 p. 380 - 390
反应条件
1: 78 percent / azoisobutyronitrile (AIBN), Bu3SnH / 55 - 65 °C 2: 92 percent / aq. NaOH / 1 h / Heating 3: 63 percent / CrO3, aq. AcOH / 26 h / 0 - 20 °C View Scheme
参考文献
Acta Chemica Scandinavica, , vol. 47, # 4 p. 380 - 390
