N-甲苯磺酰基氮杂环丙烷合成路线 （共 27 条）
反应条件
ammonia in ethanol T=18 - 25°C; 5 h;
参考文献
Baranov, S. V.; Mochalin V. B.
Journal of Organic Chemistry USSR (English Translation), 1981 , vol. 17, p. 951 - 953
Zhurnal Organicheskoi Khimii, 1981 , vol. 17, # 5 p. 1077 - 1080
反应条件
in ethanol T=18 - 25°C; 5 h;
参考文献
Baranov, S. V.; Mochalin V. B.
Journal of Organic Chemistry USSR (English Translation), 1981 , vol. 17, p. 951 - 953
Zhurnal Organicheskoi Khimii, 1981 , vol. 17, # 5 p. 1077 - 1080
反应条件
carbon dioxide; DBN; lithium iodide in toluene T=90°C; 5 h; Inert atmosphere;
参考文献
Wu, Yichen; Liu, Guosheng
Tetrahedron Letters, 2011 , vol. 52, # 48 p. 6450 - 6452
反应条件
n-butyllithium
1.) Et2O, hexane, -70 deg C to r.t.; 2.) toluene, r.t., 1 d; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Onistschenko, Andreas; Stamm, Helmut
Chemische Berichte, 1989 , vol. 122, p. 2397 - 2398
反应条件
chloro-trimethyl-silane; tetrabutyl ammonium fluoride in tetrahydrofuran
T=40°C; Ring cleavage; 12 h;
参考文献
Wu, Jie; Hou, Xue-Long; Dai, Li-Xin
Journal of Organic Chemistry, 2000 , vol. 65, # 5 p. 1344 - 1348
反应条件
magnesium in tetrahydrofuran
参考文献
Stamm, Helmut; Onistschenko, Andreas; Buchholz, Berthold; Mall, Thomas
Journal of Organic Chemistry, 1989 , vol. 54, # 1 p. 193 - 199
反应条件
water; caesium carbonate; bis(dibenzylideneacetone)-palladium(0); tri-cyclo-hexyl-phosphine in toluene
参考文献
Duda, Megan L.; Michael, Forrest E.
Journal of the American Chemical Society, 2013 , vol. 135, # 49 p. 18347 - 18349
