3-(3,5-二叔丁基-4-羟基苯基)-1-丙醇合成路线 （共 17 条）
反应条件
lithium aluminium tetrahydride in tetrahydrofuran Reduction; Heating;
参考文献
Bebbington, David; Monck, Nathaniel J. T.; Gaur, Suneel; Palmer, Alan M.; Benwell, Karen; Harvey, Victoria; Malcolm, Craig S.; Porter, Richard H. P.
Journal of Medicinal Chemistry, 2000 , vol. 43, # 15 p. 2779 - 2782
反应条件
1: 98 percent / H2 / Pd/C / ethanol / 3 h / 20 °C / 2585.81 Torr 2: 100 percent / LiAlH4 / tetrahydrofuran / Heating View Scheme
参考文献
Bebbington, David; Monck, Nathaniel J. T.; Gaur, Suneel; Palmer, Alan M.; Benwell, Karen; Harvey, Victoria; Malcolm, Craig S.; Porter, Richard H. P.
Journal of Medicinal Chemistry, 2000 , vol. 43, # 15 p. 2779 - 2782
参考文献
Iolab Corporation
Patent: US4611061 A1, 1986 ;
反应条件
1: 2,6-di-tert-butyl-phenol With sodium hydroxide T=130°C; 2 h; AutoclaveInert atmosphere; 2: allyl alcohol T=160 - 180°C; 2.5 h; AutoclaveInert atmosphere; Further stages;
参考文献
Krysin; Khalikova; Khlebnikova; Nogina; Mamatyuk
Russian Journal of General Chemistry, 2010 , vol. 80, # 11 p. 2290 - 2297
参考文献
Krysin; Khalikova; Khlebnikova; Nogina; Mamatyuk
Russian Journal of General Chemistry, 2010 , vol. 80, # 11 p. 2290 - 2297
反应条件
zinc oxide; sodium hydroxide T=180°C; 5 h; Autoclave;
参考文献
Krysin; Pustovskikh; Koptyug
Russian Journal of General Chemistry, 2010 , vol. 80, # 10 p. 2001 - 2006
反应条件
potassium hydroxide T=140°C; 10 h; Autoclave;
参考文献
Krysin; Khalikova; Khlebnikova; Nogina; Mamatyuk
Russian Journal of General Chemistry, 2010 , vol. 80, # 11 p. 2290 - 2297
反应条件
H6PMo9V3O40 in benzene T=70°C; 15 h;
参考文献
Journal of Organic Chemistry USSR (English Translation), , vol. 27, # 6.2 p. 1153 - 1156
Zhurnal Organicheskoi Khimii, , vol. 27, # 6 p. 1321 - 1325
参考文献
Prosenko; Skorobogatov; Dyubchenko; Pinko; Kandalintseva; Shakirov; Pokrovsky
Russian Chemical Bulletin, 2007 , vol. 56, # 6 p. 1119 - 1124
反应条件
T=280 - 300°C; 24 h; Inert atmosphere;
参考文献
Russian Journal of General Chemistry, , vol. 80, # 2 p. 275 - 283
