4-(溴甲基)-2,2-二甲基-1,3-二氧戊环合成路线 （共 12 条）
反应条件
sulfuric acid in acetone
参考文献
Wake Forest University
Patent: US5614548 A1, 1997 ;
反应条件
tin(IV) chloride in tetrachloromethane 2.5 h; Ambient temperature;
参考文献
Sugai; Ikawa; Hasegawa; Yoshida; Kutsuma; Akaboshi
Chemical and Pharmaceutical Bulletin, 1984 , vol. 32, # 3 p. 967 - 976
反应条件
sulfuric acid 24 h; Ambient temperature;
参考文献
Marasco Jr.; Piantadosi; Meyer; Morris-Natschke; Ishaq; Small; Daniel
Journal of Medicinal Chemistry, 1990 , vol. 33, # 3 p. 985 - 992
反应条件
toluene-4-sulfonic acid
参考文献
Fronza, Giovanni; Fuganti, Claudio; Grasselli, Piero; Servi, Stefano
Journal of Organic Chemistry, 1987 , vol. 52, # 10 p. 2086 - 2089
反应条件
ethyl bromide 2 h; Heating;
参考文献
Kolodyazhnaya; Kukhar'; Kolodyazhnyi
Russian Journal of General Chemistry, 2008 , vol. 78, # 12 p. 2407 - 2408
反应条件
Unter vermindertem Druck;
参考文献
Corbett; Kenner
Journal of the Chemical Society, 1953 , p. 3572,3574
参考文献
Corbett; Kenner
Journal of the Chemical Society, 1953 , p. 3572,3574
反应条件
sulfuric acid in ethanol Heating;
参考文献
Muramatsu,T.; Hara,I.
Bulletin de la Societe Chimique de France, 1971 , p. 3335 - 3338
反应条件
in tetrahydrofuran T=-40°C; 16 h;
参考文献
Fronza, Giovanni; Fuganti, Claudio; Grasselli, Piero; Servi, Stefano
Journal of Organic Chemistry, 1987 , vol. 52, # 10 p. 2086 - 2089
反应条件
sodium hydroxide in ethanol
T=40 - 50°C; 10 h;
参考文献
Malina, E.V.; Serebrennikova, G.A.; Evstigneeva, R.P.
Journal of Organic Chemistry USSR (English Translation), 1982 , vol. 18, p. 840 - 841
Zhurnal Organicheskoi Khimii, 1982 , vol. 18, # 5 p. 967 - 970
