反应条件
1: 74 percent / complex of CuI with 2,2'-bipyridyl / tetrahydrofuran / 1) 2 deg C, 2 h, 2) 20 deg C, 15 h 2: 1) ozone-oxygen mixture, 2) H2 / 2) Pd-CaCO3-PbO / 1) methanol, 0 deg C, 2) methanol, RT, 25 h 3: 85 percent / p-TsOH / methanol; H2O / 20 h / Ambient temperature 4: 91 percent / pyridinium chlorochromate / CH2Cl2 / 2 h / Ambient temperature View Scheme
参考文献
Odinokov, V. N.; Ishmuratov, G. Yu.; Ladenkova, I. M.; Tolstikov, G. A.
Chemistry of Natural Compounds, 1986 , vol. 22, p. 595 - 597
Khimiya Prirodnykh Soedinenii, 1986 , # 5 p. 632 - 634
