potassium tert-butylate; acide acetohydroxamique in N,N-dimethyl-formamide T=20°C; 5.5 h;

hydrogenchloride in ethanol 0.75 h; Heating;

1: acetaldehyde oxime With potassium tert-butylate in DMF (N,N-dimethyl-formamide) T=20°C; Shutske's synthesis; 0.5 h; 2: 2-fluoro-benzonitrile in DMF (N,N-dimethyl-formamide) T=20°C; 1 h; 3: With hydrogenchloride; potassium carbonate; ammonium chloride more than 3 stages;

potassium tert-butylate in N,N-dimethyl-formamide

1: potassium tert-butylate / tetrahydrofuran / 0.67 h / 95 °C / |Microwave irradiation 2: trifluoroacetic acid; hydrogenchloride / water / 0.13 h / 95 °C / |Microwave irradiation View Scheme

sodium ethanolate

暂无反应条件数据

acetic acid; zinc in water T=70°C; 12 h; Product distribution; Further Variations:Reagents;