2-(甲基硫代)-6-硝基-1,3-苯并噻唑合成路线 (共 13 条)
参考文献
The Perkin-Elmer Corporation
Patent: US6080868 A1, 2000 ;
反应条件
in water; N,N-dimethyl-formamide
参考文献
Cutter; Golden
Journal of the American Chemical Society, 1947 , vol. 69, p. 831
反应条件
1: Na2SO3; aqueous NaOH 2: NaOH; aqueous O-butyl-diethylene glycol View Scheme
参考文献
Cutter; Golden
Journal of the American Chemical Society, 1947 , vol. 69, p. 831
反应条件
1: Nitrieren 2: methanol. NaOH View Scheme
参考文献
Takahashi; Numata
Yakugaku Zasshi, 1946 , vol. 66, p. Ausg. B, S. 75
Chem.Abstr., 1952 , p. 112
参考文献
Takahashi; Numata
Yakugaku Zasshi, 1946 , vol. 66, p. Ausg. B, S. 75
Chem.Abstr., 1952 , p. 112
反应条件
2: methanol View Scheme
参考文献
Hasan; Hunter
Journal of the Chemical Society, 1936 , p. 1672,1674
参考文献
Mohanty,S. et al.
Indian Journal of Chemistry, 1968 , vol. 6, p. 136 - 139
反应条件
potassium permanganate; acetic acid
参考文献
Suzuki; Kadoya; Dohmori
Chemical and Pharmaceutical Bulletin, 1976 , vol. 24, # 5 p. 1050 - 1058
反应条件
1: acetic acid; aqueous KMnO4 2: aq.-ethanolic HCl View Scheme
参考文献
Suzuki; Kadoya; Dohmori
Chemical and Pharmaceutical Bulletin, 1976 , vol. 24, # 5 p. 1050 - 1058
反应条件
1: aq. KMnO4 / acetic acid 2: aq. NaOH 3: K2CO3 / ethanol / Heating 4: Fe, aq. HCl / ethanol 5: 3 h / 90 - 100 °C 6: (i) biphenyl, diphenyl ether, (ii) /BRN= 505934/, K2CO3, DMF 7: aq. HCl, AcOH / Heating View Scheme
参考文献
Suzuki; Kadoya; Dohmori
Chemical and Pharmaceutical Bulletin, 1976 , vol. 24, # 5 p. 1050 - 1058