反应条件
1: 96.5 percent / acetyl chloride / 5 h / 40 °C 2: 2.) H2O / 1.) THF, ether, 10 min; 2.) THF, ether, 12 h 3: 1.) 1 M LiEt3BH; 2.) 3 M NaOH, 30 percent H2O2 / 1.) THF, 0 deg C, 30 h; 2.) 30 h, RT, water 4: 28 percent / PBr3 / diethyl ether / 12 h / 40 °C 5: vitamin B12s / H2O / 0.25 h View Scheme
参考文献
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), , p. 61 - 70
