2’,3’邻异亚丙基尿苷合成路线 (共 52 条)
反应条件
1: N,N-dimethylaminopyridine 2: 83 percent / Et3N / methanol; H2O 3: 79 percent View Scheme
参考文献
Magnetic Resonance in Chemistry, , vol. 23, # 11 p. 885 - 894
反应条件
1: H2(17)O (54.75percent) / CHCl3 2: 83 percent / Et3N / methanol; H2O 3: 79 percent View Scheme
参考文献
Magnetic Resonance in Chemistry, , vol. 23, # 11 p. 885 - 894
反应条件
1: 92 percent / NaOH; pyridine 2: 85 percent / benzyl alcohol / 30 h / 90 °C View Scheme
参考文献
Carbohydrate Research, , vol. 337, # 4 p. 369 - 372
反应条件
1: 1.) ZnCl2, 2.) NaCNBH3 / 1.) MeOH, RT, 20 min, 2.) MeOH, RT, 36 h 2: 9 percent / 2.67 h / 195 - 200 °C / 5 Torr View Scheme
参考文献
Bioorganic Chemistry, , vol. 22, # 4 p. 405 - 420
反应条件
Yield given. Multistep reaction;
参考文献
Chemical and Pharmaceutical Bulletin, , vol. 35, # 8 p. 3227 - 3234
反应条件
2: 95 percent / Na2S2O4, aq. NaHCO3 / 0.25 h / 95 °C View Scheme
参考文献
Journal of the Chemical Society, Chemical Communications, , # 19 p. 1488 - 1489
反应条件
Yield given. Multistep reaction;
参考文献
Chemical and Pharmaceutical Bulletin, , vol. 35, # 8 p. 3227 - 3234
反应条件
sodium hydroxide T=90.1°C; various reagent concentration, decomposition to nonchromophoric products; Rate constantMechanism;
参考文献
Acta Chemica Scandinavica, Series B: Organic Chemistry and Biochemistry, , vol. 40, # 10 p. 798 - 805
反应条件
T=190 - 200°C; P=5 Torr; 0.5 h; other thymidine derivatives, var. time; Mechanism;
参考文献
Bioorganic Chemistry, , vol. 22, # 4 p. 405 - 420
参考文献
Nucleosides and Nucleotides, , vol. 17, # 1-3 p. 161 - 173