4-O-(2,3,4,6-四-O-乙酰基)-β-D-吡喃(型)葡糖基-D-吡喃(型)葡糖四乙酸酯合成路线 (共 38 条)
反应条件
sodium acetate Reflux;
参考文献
Journal of the American Chemical Society, , vol. 135, # 24 p. 9055 - 9077
反应条件
H-Beta zeolite 7 h; Ambient temperature; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Synlett, , # 1 p. 129 - 131
反应条件
molybdenum dichloride dioxide; acetic acid T=20°C;
参考文献
Liu, Cheng-Yuan; Chen, Hui-Ling; Ko, Chih-Min; Chen, Chien-Tien
Tetrahedron, 2011 , vol. 67, # 5 p. 872 - 876
参考文献
Xu, Peng; Yang, Jacqueline Y.; Kovac, Pavol
Journal of Carbohydrate Chemistry, 2012 , vol. 31, # 9 p. 711 - 720
反应条件
boron trifluoride diethyl etherate in toluene T=22°C; 3 h; Yield given;
参考文献
Journal of Organic Chemistry, , vol. 53, # 24 p. 5629 - 5647
反应条件
1: 1.) HgO, HgBr2, CaSO4, 2.) HgBr2 / 1.) CHCl3, 20 h, 2.) toluene, nitromethane, 50 deg C, 24 h 2: BF3*Et2O / toluene / 3 h / 22 °C View Scheme
参考文献
Journal of Organic Chemistry, , vol. 53, # 24 p. 5629 - 5647
反应条件
0.5 h; Heating / reflux;
参考文献
EP1787661 A1, ;
Page/Page column 14 ;
反应条件
sodium acetate T=110°C;
参考文献
Monatshefte fuer Chemie, , vol. 55, p. 25,26, 30
反应条件
boron trifluoride diethyl etherate in toluene 2 h; Ambient temperature; Yield given. Yields of byproduct given;
参考文献
Tetrahedron Letters, , vol. 27, # 6 p. 753 - 756
反应条件
potassium acetate 0.0833333 h; Inert atmosphereReflux;
参考文献
Helvetica Chimica Acta, , vol. 95, # 12 p. 2652 - 2659