5-氨基-2-(苯基硫基)苯甲酸甲酯合成路线 （共 4 条）
反应条件
iron; acetic acid T=80°C;
参考文献
Parlow, John J.; Stevens, Anna M.; Stegeman, Roderick A.; Stallings, William C.; Kurumbail, Ravi G.; South, Michael S.
Journal of Medicinal Chemistry, 2003 , vol. 46, # 20 p. 4297 - 4312
反应条件
1: 87 percent / Et3N / tetrahydrofuran / 20 h / Heating 2: oxalyl chloride; DMF / CH2Cl2 / 20 °C 3: 4.21 g / pyridine / CH2Cl2 / 20 °C 4: 75 percent / Fe; glacial AcOH / 80 °C View Scheme
参考文献
Parlow, John J.; Stevens, Anna M.; Stegeman, Roderick A.; Stallings, William C.; Kurumbail, Ravi G.; South, Michael S.
Journal of Medicinal Chemistry, 2003 , vol. 46, # 20 p. 4297 - 4312
反应条件
1: oxalyl chloride; DMF / CH2Cl2 / 20 °C 2: 4.21 g / pyridine / CH2Cl2 / 20 °C 3: 75 percent / Fe; glacial AcOH / 80 °C View Scheme
参考文献
Parlow, John J.; Stevens, Anna M.; Stegeman, Roderick A.; Stallings, William C.; Kurumbail, Ravi G.; South, Michael S.
Journal of Medicinal Chemistry, 2003 , vol. 46, # 20 p. 4297 - 4312
反应条件
1: 87 percent / Et3N / tetrahydrofuran / 20 h / Heating 2: oxalyl chloride; DMF / CH2Cl2 / 20 °C 3: 4.21 g / pyridine / CH2Cl2 / 20 °C 4: 75 percent / Fe; glacial AcOH / 80 °C View Scheme
参考文献
Parlow, John J.; Stevens, Anna M.; Stegeman, Roderick A.; Stallings, William C.; Kurumbail, Ravi G.; South, Michael S.
Journal of Medicinal Chemistry, 2003 , vol. 46, # 20 p. 4297 - 4312
