4-叔丁基-5-甲氧基-邻苯醌合成路线 （共 17 条）
反应条件
potassium dihydrogenphosphate; Fremy’s salt in water; acetone
参考文献
Lam; Garg; Swanson; Pezzuto
Journal of Pharmaceutical Sciences, 1988 , vol. 77, # 5 p. 393 - 395
反应条件
lead dioxide in methanol T=15 - 20°C; Yield given. Yields of byproduct given;
参考文献
Demmin, Timothy R.; Rogic, Milorad M.
Journal of Organic Chemistry, 1980 , vol. 45, # 21 p. 4210 - 4214
反应条件
sodium hydroxide in methanol T=20°C; 0.166667 h;
参考文献
Fujita, Shinsaku
Journal of Organic Chemistry, 1983 , vol. 48, # 2 p. 177 - 183
反应条件
1: 96 percent / 35percent HCl / ethanol / 1 h / Heating 2: pyridine / N,N-dimethyl-acetamide / 2 h / Ambient temperature 3: 57 percent / MnO2 / acetone 4: 1 N sodium hydroxide / 0.5 h / Ambient temperature View Scheme
参考文献
Fujita, Shinsaku
Journal of Organic Chemistry, 1983 , vol. 48, # 2 p. 177 - 183
反应条件
1: pyridine / N,N-dimethyl-acetamide / 2 h / Ambient temperature 2: 57 percent / MnO2 / acetone 3: 1 N sodium hydroxide / 0.5 h / Ambient temperature View Scheme
参考文献
Fujita, Shinsaku
Journal of Organic Chemistry, 1983 , vol. 48, # 2 p. 177 - 183
反应条件
1: 57 percent / MnO2 / acetone 2: 1 N sodium hydroxide / 0.5 h / Ambient temperature View Scheme
参考文献
Fujita, Shinsaku
Journal of Organic Chemistry, 1983 , vol. 48, # 2 p. 177 - 183
反应条件
2: 62 percent / MnO2 / acetone / 1.5 h / Ambient temperature 3: 1 N sodium hydroxide / methanol / 0.17 h / 20 °C View Scheme
参考文献
Fujita, Shinsaku
Journal of Organic Chemistry, 1983 , vol. 48, # 2 p. 177 - 183
反应条件
1: 62 percent / MnO2 / acetone / 1.5 h / Ambient temperature 2: 1 N sodium hydroxide / methanol / 0.17 h / 20 °C View Scheme
参考文献
Fujita, Shinsaku
Journal of Organic Chemistry, 1983 , vol. 48, # 2 p. 177 - 183
反应条件
1: 88 percent / sodium methoxide 2: 96 percent / 35percent HCl / ethanol / 1 h / Heating 3: pyridine / N,N-dimethyl-acetamide / 2 h / Ambient temperature 4: 57 percent / MnO2 / acetone 5: 1 N sodium hydroxide / 0.5 h / Ambient temperature View Scheme
参考文献
Fujita, Shinsaku
Journal of Organic Chemistry, 1983 , vol. 48, # 2 p. 177 - 183
反应条件
nitrogen(IV) oxide in dichloromethane T=-50°C; Irradiation;
参考文献
Svensson, Jan Olof
Acta Chemica Scandinavica, 1997 , vol. 51, # 1 p. 31 - 36
