(吡啶-2-基亚甲基氨基)硫脲合成路线 （共 12 条）
反应条件
acetic acid in ethanol 10 h; Reflux;
参考文献
Yi, Wei; Dubois, Carole; Yahiaoui, Samir; Haudecoeur, Romain; Belle, Catherine; Song, Huacan; Hardre, Renaud; Reglier, Marius; Boumendjel, Ahcne
European Journal of Medicinal Chemistry, 2011 , vol. 46, # 9 p. 4330 - 4335
反应条件
disodium tetrasulfide T=110°C;
参考文献
Wegler et al.
Angewandte Chemie, 1958 , vol. 70, p. 351,365
反应条件
sodium carbonate; glycerol
参考文献
Fox
Journal of Organic Chemistry, 1952 , vol. 17, p. 547,553
反应条件
1: pyridine 2: sodium carbonate; glycerol View Scheme
参考文献
Supaniewski et al.
Bulletin de l'Academie Polonaise des Sciences, Serie des Sciences Chimiques, 1955 , vol. 3, p. 55,58
Chem.Abstr., 1956 , # 7800
反应条件
1: lead (IV)-acetate; benzene 2: water; ethanol; acetic acid View Scheme
参考文献
Micovic; Mihailovic
Recueil des Travaux Chimiques des Pays-Bas, 1952 , vol. 71, p. 970,974
反应条件
1: diethyl ether; lithium alanate 2: lead (IV)-acetate; benzene 3: water; ethanol; acetic acid View Scheme
参考文献
Micovic; Mihailovic
Recueil des Travaux Chimiques des Pays-Bas, 1952 , vol. 71, p. 970,974
反应条件
iron(III) chloride in ethanol 2 h; Heating;
参考文献
Turner, Stephen; Myers, Malcolm; Gadie, Brian; Nelson, Anthony J.; Pape, Robin; et al.
Journal of Medicinal Chemistry, 1988 , vol. 31, # 5 p. 902 - 906
反应条件
1: FeCl3*6H2O / ethanol / 2 h / Heating
2: conc. HCl, aq. NaNO2, copper, glacial acetic acid / 4 h / 15 - 20 °C
View Scheme
参考文献
Turner, Stephen; Myers, Malcolm; Gadie, Brian; Nelson, Anthony J.; Pape, Robin; et al.
Journal of Medicinal Chemistry, 1988 , vol. 31, # 5 p. 902 - 906
反应条件
in ethanol; water
addn. of Cu(2+)-salt to an aq.-alc. soln. of C7H8N4S buffered with acetate;; ppt.;;
参考文献
Gmelin Handbook: Cu: MVol.B4, 209, page 1911 - 1913
参考文献
Kubota, Seiju; Ueda, Yasufumi; Fujikane, Kazuichi; Toyooka, Kouhei; Shibuya, Masayuki
Journal of Organic Chemistry, 1980 , vol. 45, # 8 p. 1473 - 1477
