3,4-二(三氟甲基)二硫环丁烯合成路线 （共 10 条）
反应条件
at 225°C, under pressure; at 200°C in presence of iodine;
参考文献
Krespan,C.G.
Journal of the American Chemical Society, 1961 , vol. 83, p. 3434 - 3437
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Gmelin Handbook: F: PerFHalOrg.1, 1.1.5.2, page 57 - 85
参考文献
Krespan,C.G.
Journal of the American Chemical Society, 1961 , vol. 83, p. 3434 - 3437
Full Text View citing articles Show Details
Gmelin Handbook: F: PerFHalOrg.1, 1.1.5.2, page 57 - 85
反应条件
in benzene under N2, soln. of Nb complex and hexafluorobut-2-yne in benzene stirred for 7 d at 40-50°C; concd. under vac., filtered, chromd., violet soln. concd., pentane added, kept at -60°C for 20 h, filtered, dried in vac., elem. anal.;
参考文献
Migot, Jean-Louis; Sala-Pala,Jean; Guerchais, Jacques-E.
Journal of Organometallic Chemistry, 1983 , vol. 243, # 4 p. 427 - 436
反应条件
3-chloro-benzenecarboperoxoic acid Ambient temperature;
参考文献
Maletzko, Christian; Sundermeyer, Wolfgang; Pritzkow, Hans; Irngartinger, Hermann; Huber-Patz, Ursula
Chemische Berichte, 1991 , vol. 124, # 9 p. 2025 - 2031
反应条件
Decomposition; 3 h; Photolysis;
参考文献
Brownridge, Scott; Du, Hongbin; Fairhurst, Shirlcy A.; Haddon, Robert C.; Oberhammer, Heinz; Parsons, Simon; Passmore, Jack; Schriver, Melbourne J.; Sutcliffe, Leslie H.; Westwood, Nicholas P. C.
Journal of the Chemical Society, Dalton Transactions, 2000 , # 19 p. 3365 - 3382
反应条件
triethylamine or acrylnitrile
参考文献
Krespan,C.G. et al.
Journal of the American Chemical Society, 1960 , vol. 82, p. 1515 - 1516
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Krespan,C.G.
Journal of the American Chemical Society, 1961 , vol. 83, p. 3434 - 3437
View citing articles Show Details
Gmelin Handbook: F: PerFHalOrg.1, 1.1.5.2, page 57 - 85
反应条件
byproducts: S; 130°C;
参考文献
Krespan,C.G.
Journal of the American Chemical Society, 1961 , vol. 83, p. 3434 - 3437
View citing articles Show Details
Gmelin Handbook: F: PerFHalOrg.1, 1.1.5.2, page 57 - 85
反应条件
in cyclohexane
125°C; 8 h;
参考文献
Gmelin Handbook: F: PerFHalOrg.1, 1.1.5.2, page 57 - 85
参考文献
Gmelin Handbook: F: PerFHalOrg.1, 1.1.5.2, page 57 - 85
反应条件
in dichloromethane
T=-78°C;
参考文献
Gmelin Handbook: F: PerFHalOrg.SVol.2, 6.2.1.5.1.2, page 15 - 38
