二(三氟甲基)砷烷基-二(三氟甲基)砷合成路线 （共 16 条）
反应条件
Hg in Carius tube; large excess of Hg; 20°C, 48 h;
参考文献
Brandt, G. R. A.; Emeleus, H. J.; Haszeldine, R. N.
Journal of the Chemical Society, 1952 , p. 2552 - 2555
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Gmelin Handbook: F: PerFHalOrg.3, 2.9, page 222 - 225
反应条件
mercury in Carius tube; large excess of Hg; 20°C, 24 h;
参考文献
Gmelin Handbook: F: PerFHalOrg.3, 2.9, page 222 - 225
反应条件
hydrogenchloride; mercury in Carius tube at 23°C (17 h); fractionated condensation;
参考文献
Gmelin Handbook: F: PerFHalOrg.3, 2.2, page 191 - 196
参考文献
Singh,J.; Burg,A.B.
Journal of the American Chemical Society, 1966 , vol. 88, p. 718 - 722
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Gmelin Handbook: F: PerFHalOrg.3, 2.9, page 222 - 225
反应条件
Cu; Zn; hydrochloric acid intensive shaking; further addn. of HCl during 1 h; fractionated condensation with N2 carrier gas;
参考文献
Emeleus, H. J.; Haszeldine, R. N.; Walaschewski, E. G.
Journal of the Chemical Society, 1953 , p. 1552 - 1564
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Gmelin Handbook: F: PerFHalOrg.3, 2.2, page 191 - 196
反应条件
byproducts: P-O compounds; 25°C (72 h); (CF3)2PCl in no excess;
参考文献
Singh,J.; Burg,A.B.
Journal of the American Chemical Society, 1966 , vol. 88, p. 718 - 722
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Gmelin Handbook: F: PerFHalOrg.3, 2.3, page 196 - 200
参考文献
Gmelin Handbook: F: PerFHalOrg.3, 2.9, page 222 - 225
参考文献
Gmelin Handbook: F: PerFHalOrg.3, 2.2, page 191 - 196
参考文献
Gmelin Handbook: F: PerFHalOrg.3, 2.2, page 191 - 196
参考文献
Gmelin Handbook: F: PerFHalOrg.3, 2.2, page 191 - 196
