3-硝基甲基-2-苯并呋喃-1(3H)-酮合成路线 （共 5 条）
反应条件
sodium hydroxide in water; methanol hydrate
反应条件
sodium hydroxide in methanol 2.5 h; Ambient temperature;
参考文献
Hauser, Frank M.; Baghdanov, Vaceli M.
Journal of Organic Chemistry, 1988 , vol. 53, # 20 p. 4676 - 4681
参考文献
Archiv der Pharmazie (Weinheim, Germany), , vol. 275, p. 397,404
Magyar gyogysz. Tars. Ert., , vol. 13, p. 680,684
Chem. Zentralbl., , vol. 108, # II p. 2345
Journal of Organic Chemistry, , vol. 10, p. 429,434
反应条件
hydrogenchloride; hydrogen; palladium on activated charcoal in methanol P=3040 Torr;
参考文献
Donati, Cosimo; Prager, Rolf H.; Weber, Ben
Australian Journal of Chemistry, 1989 , vol. 42, # 6 p. 787 - 795
反应条件
1: 93 percent / NaBH4 / dimethylsulfoxide / 1 h / Ambient temperature
2: 1.) NaOCH3, TiCl3, CH3CO2NH4, 6 N aq. HCl, 2.) Ac2O, HClO4 / 1.) THF, RT, 1.5 h, 2.) EtOAc, reflux, 0.5 h
View Scheme
参考文献
Hauser, Frank M.; Baghdanov, Vaceli M.
Journal of Organic Chemistry, 1988 , vol. 53, # 20 p. 4676 - 4681
