9,10-二氢-9-氧杂-10-磷杂菲-10-氧化物合成路线 (共 11 条)
反应条件
water; hydrogenchloride T=80°C; 1 h; Product distribution / selectivity;
参考文献
UFC CORPORATION
Patent: US2011/34717 A1, 2011 ;
Location in patent: Page/Page column 3 ;
反应条件
T=165°C; P=3.75038 Torr; 2.25 h;
参考文献
US2010/69657 A1, ;
Page/Page column 4-5 ;
反应条件
1: AlCl3 / heptane 2: aq. ethanol View Scheme
参考文献
J. Gen. Chem. USSR (Engl. Transl.), , vol. 42, p. 93 - 96,88 - 90
反应条件
T=160°C; Cyclization; P=30 Torr; 2 h; Activation energy;
参考文献
Phosphorus, Sulfur and Silicon and Related Elements, , vol. 139, p. 45 - 55
反应条件
phosphorus trichoride in chloroform 3 h; Inert atmosphereReflux;
参考文献
Abranyi-Balogh, Peter; Keglevich, Gyoergy
Synthetic Communications, 2011 , vol. 41, # 10 p. 1421 - 1426
反应条件
tetrakis(triphenylphosphine) palladium(0); sodium acetate in 1,4-dioxane T=100°C; 12 h; Inert atmosphere;
参考文献
Yang, Liancheng; Xu, Longhe; Tao, Zaizhou
Phosphorus, Sulfur and Silicon and the Related Elements, 2009 , vol. 184, # 12 p. 3175 - 3181
反应条件
tetrakis(triphenylphosphine) palladium(0); sodium acetate in 1,4-dioxane T=100°C; 24 h; Inert atmosphere;
参考文献
Yang, Liancheng; Xu, Longhe; Tao, Zaizhou
Phosphorus, Sulfur and Silicon and the Related Elements, 2009 , vol. 184, # 12 p. 3175 - 3181
参考文献
Wang, Xin; Hu, Yuan; Song, Lei; Xing, Weiyi; Lu, Hongdian; Lv, Pin; Jie, Ganxin
Polymer, 2010 , vol. 51, # 11 p. 2435 - 2445
参考文献
DIC Corporation
Patent: EP2409979 A1, 2012 ;
Location in patent: Page/Page column 36 ;