1,3-二(4-甲基苯基)丙烷-1,3-二酮合成路线 （共 24 条）
反应条件
sodium hydride in dimethyl sulfoxide; mineral oil T=20 - 30°C; 2 h; Inert atmosphereSealed tube;
参考文献
Zou, Liang-Hua; Priebbenow, Daniel L.; Wang, Long; Mottweiler, Jakob; Bolm, Carsten
Advanced Synthesis and Catalysis, 2013 , vol. 355, # 13 p. 2558 - 2563
反应条件
samarium (III) iodide in acetonitrile T=70°C; 3 h;
参考文献
Hao, Wenying; Zhang, Yongmin; Ying, Taokai; Lu, Pin
Synthetic Communications, 1996 , vol. 26, # 12 p. 2421 - 2427
参考文献
Ohta, Kazuchika; Muroki, Hiromitsu; Takagi, Akira; Yamamoto, Iwao; Matszaki, Kei
Molecular Crystals and Liquid Crystals (1969-1991), 1986 , vol. 135, p. 247 - 264
反应条件
[2,2']bipyridinyl; palladium (II) trifluoroacetate; water; trifluoroacetic acid in tetrahydrofuran T=80°C; 36 h; Inert atmosphereSchlenk technique;
参考文献
Wang, Xingyong; Liu, Miaochang; Xu, Long; Wang, Qingzong; Chen, Jiuxi; Ding, Jinchang; Wu, Huayue
Journal of Organic Chemistry, 2013 , vol. 78, # 11 p. 5273 - 5281
反应条件
1: 71 percent / Br2 / CHCl3 / Ambient temperature 2: 1.) KOH, 2.) HCl, water / 1.) methanol, reflux, 3 h, 2.) methanol, reflux, 2 h View Scheme
参考文献
Suman, Mrs.; Singh, Rajvir; Malik, M. S.; Kathpal, T. S.; Malik, O. P.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1995 , vol. 34, # 8 p. 743 - 746
反应条件
1: 75 percent / NaOH / ethanol; H2O / 3 h 2: 71 percent / Br2 / CHCl3 / Ambient temperature 3: 1.) KOH, 2.) HCl, water / 1.) methanol, reflux, 3 h, 2.) methanol, reflux, 2 h View Scheme
参考文献
Suman, Mrs.; Singh, Rajvir; Malik, M. S.; Kathpal, T. S.; Malik, O. P.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1995 , vol. 34, # 8 p. 743 - 746
反应条件
1: 75 percent / NaOH / ethanol; H2O / 3 h 2: 71 percent / Br2 / CHCl3 / Ambient temperature 3: 1.) KOH, 2.) HCl, water / 1.) methanol, reflux, 3 h, 2.) methanol, reflux, 2 h View Scheme
参考文献
Suman, Mrs.; Singh, Rajvir; Malik, M. S.; Kathpal, T. S.; Malik, O. P.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1995 , vol. 34, # 8 p. 743 - 746
反应条件
1: sulfuric acid / 10 h / |Reflux; |Sealed tube 2: sodium hydride / mineral oil; dimethyl sulfoxide / 2 h / 20 - 30 °C / |Inert atmosphere; |Sealed tube View Scheme
参考文献
Zou, Liang-Hua; Priebbenow, Daniel L.; Wang, Long; Mottweiler, Jakob; Bolm, Carsten
Advanced Synthesis and Catalysis, 2013 , vol. 355, # 13 p. 2558 - 2563
反应条件
aluminium trichloride
参考文献
Behal; Auger
Bulletin de la Societe Chimique de France, 1893 , vol. <3> 9, p. 699
反应条件
(i) AlCl3, (ii) aq. HCl; Multistep reaction;
参考文献
Dayer,F. et al.
Helvetica Chimica Acta, 1974 , vol. 57, # 7 p. 2201 - 2209
