二噻吩[3,2-B:2',3'-D]噻吩合成路线 （共 19 条）
反应条件
copper in quinoline T=230°C;
参考文献
Frey, Joseph; Bond, Andrew D.; Holmes, Andrew B.
Chemical Communications, 2002 , # 20 p. 2424 - 2425
反应条件
1: With n-butyllithium in diethyl ether T=-78°C; 0.666667 h; 2: With (PhSO2)2S in diethyl ether T=-78 - 20°C;
参考文献
Allared, Fredrik; Hellberg, Jonas; Remonen, Tommi
Tetrahedron Letters, 2002 , vol. 43, # 8 p. 1553 - 1554
反应条件
1: in diethyl ether; hexane T=-78 - 20°C; Inert atmosphere; 2: With n-butyllithium in diethyl ether; hexane T=0°C; 1.5 h; Inert atmosphereReflux; 3: With copper dichloride in diethyl ether; hexane T=0 - 20°C; Inert atmosphere;
参考文献
Chen, Ming-Chou; Chiang, Yen-Ju; Kim, Choongik; Guo, Yue-Jhih; Chen, Sheng-Yu; Liang, You-Jhih; Huang, Yu-Wen; Hu, Tarng-Shiang; Lee, Gene-Hsiang; Facchetti, Antonio; Marks, Tobin J.
Chemical Communications, 2009 , # 14 p. 1846 - 1848
反应条件
copper T=200°C; 0.75 h;
参考文献
Schroth, Werner; Hintzsche, Ekkehard; Jordan, Hartwig; Jende, Thomas; Spitzner, Roland; Thondorf, Iris
Tetrahedron, 1997 , vol. 53, # 22 p. 7509 - 7528
反应条件
1: 96 percent / aq. LiOH / tetrahydrofuran / 3 h / Heating 2: 87 percent / Cu / quinoline / 230 °C View Scheme
参考文献
Chemical Communications, , # 20 p. 2424 - 2425
反应条件
1: With n-butyllithium in light petroleum; diethyl ether T=0°C; Inert atmosphereReflux; 2: With copper dichloride in light petroleum; diethyl ether T=0 - 20°C; Inert atmosphere;
参考文献
Kim, Choongik; Chen, Ming-Chou; Chiang, Yen-Ju; Guo, Yue-Jhih; Youn, Jangdae; Huang, Hui; Liang, You-Jhih; Lin, Yu-Jou; Huang, Yu-Wen; Hu, Tarng-Shiang; Lee, Gene-Hsiang; Facchetti, Antonio; Marks, Tobin J.
Organic Electronics: physics, materials, applications, 2010 , vol. 11, # 5 p. 801 - 813
反应条件
1: 71 percent / K2CO3 / dimethylformamide / 72 h / 25 °C 2: 96 percent / aq. LiOH / tetrahydrofuran / 3 h / Heating 3: 87 percent / Cu / quinoline / 230 °C View Scheme
参考文献
Chemical Communications, , # 20 p. 2424 - 2425
反应条件
n-butyllithium; (PhSO2)2S; copper dichloride Yield given. Multistep reaction;
参考文献
Journal of the American Chemical Society, , vol. 120, # 9 p. 2206 - 2207
反应条件
hydrogen sulfide T=500°C; Product distribution;
参考文献
Chemistry of Heterocyclic Compounds (New York, NY, United States), , vol. 22, # 12 p. 1301 - 1306
Khimiya Geterotsiklicheskikh Soedinenii, , vol. 22, # 12 p. 1614 - 1619
反应条件
hydrogen sulfide T=450 - 600°C; Product distribution;
参考文献
Chemistry of Heterocyclic Compounds (New York, NY, United States), , vol. 22, # 12 p. 1301 - 1306
Khimiya Geterotsiklicheskikh Soedinenii, , vol. 22, # 12 p. 1614 - 1619
