H2O; H2O2 in water
byproducts: iodine; 30 min shaking with H2O at 20°C excluding air; dropwise addn. of H2O2; filtration; washing (H2O); 5-6 d freeze-drying; sublimation;
参考文献
Gmelin Handbook: F: PerFHalOrg.3, 1.6, page 40 - 51
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Bennett, F. W.; Emeleus, H. J.; Haszeldine, R. N.
Journal of the Chemical Society, 1954 , p. 3598 - 3603
Gmelin Handbook: F: PerFHalOrg.3, 1.17, page 176 - 185
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Bennet, F. W.; Emeleus, H. J.; Haszeldine, R. N.
Journal of the Chemical Society, 1953 , p. 1565 - 1571
Burg,A.B.; Nixon,J.F.
Journal of the American Chemical Society, 1964 , vol. 86, p. 356 - 357
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Gmelin Handbook: F: PerFHalOrg.3, 1.2, page 14 - 30
Gmelin Handbook: F: PerFHalOrg.3, 1.9, page 70 - 123
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Bennet, F. W.; Emeleus, H. J.; Haszeldine, R. N.
Journal of the Chemical Society, 1953 , p. 1565 - 1571