1,1,1-三氟-2,3-环氧丙烷合成路线 (共 28 条)
反应条件
copper(l) iodide in tetrahydrofuran; diethyl ether 1.) -20 to 25 deg C, 2.) 25 deg C, 3 h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Ramachandran, P. Veeraraghavan; Gong, Baoqing; Brown, Herbert C.
Journal of Organic Chemistry, 1995 , vol. 60, # 1 p. 41 - 46
反应条件
Yield given. Multistep reaction;
参考文献
Ramachandran, P. Veeraraghavan; Gong, Baoqing; Brown, Herbert C.
Journal of Organic Chemistry, 1995 , vol. 60, # 1 p. 41 - 46
反应条件
lithium aluminium tetrahydride in diethyl ether T=25°C; 1.5 h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Ramachandran, P. Veeraraghavan; Gong, Baoqing; Brown, Herbert C.
Journal of Organic Chemistry, 1995 , vol. 60, # 1 p. 41 - 46
反应条件
lithium aluminium tetrahydride in diethyl ether T=25°C; 1.5 h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Ramachandran, P. Veeraraghavan; Gong, Baoqing; Brown, Herbert C.
Journal of Organic Chemistry, 1995 , vol. 60, # 1 p. 41 - 46
反应条件
copper(l) iodide in tetrahydrofuran; diethyl ether 1.) -20 to 25 deg C, 2.) 25 deg C, 3 h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Ramachandran, P. Veeraraghavan; Gong, Baoqing; Brown, Herbert C.
Journal of Organic Chemistry, 1995 , vol. 60, # 1 p. 41 - 46
参考文献
McBee et al.
Journal of the American Chemical Society, 1956 , vol. 78, p. 3851,3853
反应条件
sodium hydrogencarbonate in ethyl acetate
参考文献
Mitsui Chemicals, Inc.
Patent: US6180800 B2, 2001 ;
参考文献
Voronkov,M.G. et al.
J. Gen. Chem. USSR (Engl. Transl.), 1978 , vol. 48, p. 2238 - 2245,2033 - 2038