1,1,1-三氟-2,3-环氧丙烷合成路线 （共 28 条）
反应条件
sodium hydroxide T=100°C;
参考文献
Dunn, Caroline; Gibson, Colin L.; Suckling, Colin J.
Tetrahedron, 1996 , vol. 52, # 40 p. 13017 - 13026
反应条件
sodium hydroxide T=85°C;
参考文献
Ramachandran, P. Veeraraghavan; Padiya, Kamlesh J.
Journal of Fluorine Chemistry, 2007 , vol. 128, # 10 p. 1255 - 1259
反应条件
sodium hydroxide in water T=100°C; Title compound not separated from byproducts.;
参考文献
Journal of Fluorine Chemistry, , vol. 128, # 10 p. 1255 - 1259
反应条件
1: With N-bromosuccinmide; sulfuric acid; acetic acid T=65 - 70°C; 11 h; 2: With sodium hydroxide in water T=120 - 130°C;
参考文献
Lermontov, S. A.; Kuryleva, N. V.; Velikokhat'ko, T. N.
Russian Chemical Bulletin, 2002 , vol. 51, # 3 p. 550 - 551
Izvestiya Akademi Nauk, Seriya Khimicheskaya, 2002 , # 3 p. 508 - 509
反应条件
Nitrous oxide T=20 - 300°C; P=750.075 Torr; 4 h; Inert atmosphere; Kinetics; Reagent/catalyst;
参考文献
Journal of Catalysis, , vol. 312, p. 139 - 151
反应条件
ammonia in water T=20°C; 22 h;
参考文献
ASTRAZENECA AB; SCHERING AG
Patent: WO2007/46747 A1, 2007 ;
Location in patent: Page/Page column 29 ;
WO 2007/046747 A1
反应条件
T=403.9 - 467.9°C; P=6 - 105 Torr; Heating; Kinetics;
参考文献
Flowers, Michael C.; Honeyman, Malcolm R.
Journal of the Chemical Society, Faraday Transactions 1: Physical Chemistry in Condensed Phases, 1980 , vol. 76, p. 2290 - 2295
反应条件
lithium aluminium tetrahydride; diethyl ether
参考文献
Groth,R.H.
Journal of Organic Chemistry, 1960 , vol. 25, p. 102 - 105
反应条件
T=403.9 - 467.9°C; P=6 - 105 Torr; Heating; Kinetics;
参考文献
Flowers, Michael C.; Honeyman, Malcolm R.
Journal of the Chemical Society, Faraday Transactions 1: Physical Chemistry in Condensed Phases, 1980 , vol. 76, p. 2290 - 2295
反应条件
trifluorormethanesulfonic acid in dichloromethane T=0 - 20°C; Friedel-Crafts alkylation;
参考文献
Prakash, G. K. Surya; Linares-Palomino, Pablo J.; Glinton, Kevin; Chacko, Sujith; Rasul, Golam; Mathew, Thomas; Olah, George A.
Synlett, 2007 , # 7 p. 1158 - 1162
