1-氟-1,2,2-三氯乙烷合成路线 （共 32 条）
反应条件
antimony(V) pentachloride; SbF3 T=130 - 140°C;
参考文献
Whalley
Journal of the Society of Chemical Industry, London, 1947 , vol. 66, p. 429
反应条件
bromine trifluoride; tin(IV) chloride in 1,2,2-trifluoro-trichloroethane T=20 - 25°C;
参考文献
Kartashov, A. V.; Chuvatkin, N. N.; Boguslavskaya, L. S.
Journal of Organic Chemistry USSR (English Translation), 1988 , vol. 24, # 12 p. 2276 - 2278
Zhurnal Organicheskoi Khimii, 1988 , vol. 24, # 12 p. 2522 - 2525
反应条件
fluoro chloride in 1,2,2-trifluoro-trichloroethane; ethyl acetate T=20 - 25°C; 0.5 h;
参考文献
Boguslavskaya, L. S.; Chuvatkin, N. N.; Panteleeva, I. Yu.
Journal of Organic Chemistry USSR (English Translation), 1982 , vol. 18, # 10 p. 1832 - 1842
Zhurnal Organicheskoi Khimii, 1982 , vol. 18, # 10 p. 2082 - 2094
反应条件
MeOCl; boron trifluoride diethyl etherate in dichloromethane T=25°C; 0.0833333 h; Yield given;
参考文献
Heasley, Victor L.; Gipe, Robert K.; Martin, Jody L.; Wiese, Harry C.; Oakes, Melanie L.; Shellhamer, Dale F.
Journal of Organic Chemistry, 1983 , vol. 48, # 19 p. 3195 - 3199
反应条件
chlorine unter Belichtung;
参考文献
Hauptschein; Bigelow
Journal of the American Chemical Society, 1951 , vol. 73, p. 5591
反应条件
fluoro chloride in 1,2,2-trifluoro-trichloroethane
参考文献
Boguslavskaya, L. S.; Chuvatkin, N. N.; Panteleeva, I. Yu.
Journal of Organic Chemistry USSR (English Translation), 1982 , vol. 18, # 10 p. 1832 - 1842
Zhurnal Organicheskoi Khimii, 1982 , vol. 18, # 10 p. 2082 - 2094
反应条件
in monofluoro-trichloromethane T=-111 - 22°C; 20 h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Johri, Kamalesh K.; DesMarteau, Darryl D.
Journal of Organic Chemistry, 1983 , vol. 48, # 2 p. 242 - 250
反应条件
hydrogen fluoride; hexachloromelamine in methanol; chloroform
参考文献
Boguslavskaya,L.S. et al.
Journal of Organic Chemistry USSR (English Translation), 1975 , vol. 11, # 2 p. 252 - 256
Zhurnal Organicheskoi Khimii, 1975 , p. 257 - 262
反应条件
hydrogen fluoride; hexachloromelamine in methanol; chloroform
参考文献
Boguslavskaya,L.S. et al.
Journal of Organic Chemistry USSR (English Translation), 1975 , vol. 11, # 2 p. 252 - 256
Zhurnal Organicheskoi Khimii, 1975 , p. 257 - 262
反应条件
sulfur(IV) fluoride; hydrogen fluoride; chlorine T=20°C; 24 h; Yield given;
参考文献
Kunshenko, B. V.; Mokhamed, Nagib Mukhtar; Omarov, V. O.; Muratov, N. N.; Yagupol'skii, L. M.
Journal of Organic Chemistry USSR (English Translation), 1992 , vol. 28, # 4.1 p. 511 - 518
Zhurnal Organicheskoi Khimii, 1992 , vol. 28, # 4 p. 672 - 680
