反应条件
in neat (no solvent) equimolar amt. of BF3 and (CH3)2NH were distd. into a bulb cooled in liq. N2, the bulb was isolated and allowed to warm slowly , the react. mixt. was cooled at intervals; pumped at room temp. to remove excess reactants and volatile products;
参考文献
Kroto, Harold W.; McNaughton, Donald
Journal of the Chemical Society, Dalton Transactions: Inorganic Chemistry (1972-1999), 1985 , p. 1767 - 1770