1-叠氮-1-脱氧-β-D-吡喃半乳糖苷合成路线 （共 10 条）
反应条件
sodium methylate in methanol Inert atmosphere;
参考文献
Zeitschrift fur Naturforschung - Section B Journal of Chemical Sciences, , vol. 64, # 11-12 p. 1639 - 1652
反应条件
1: NaN3; aq. NaHCO3; TBAHS / CH2Cl2 / 2 h / 20 °C 2: NaOMe / methanol / 20 °C View Scheme
参考文献
Journal of the American Chemical Society, , vol. 127, # 50 p. 17618 - 17619
反应条件
1: 96 percent / TMSN3; SnCl4 2: 91 percent / NaOMe / methanol / 0.5 h View Scheme
参考文献
Chemistry - A European Journal, , vol. 10, # 17 p. 4240 - 4251
反应条件
benzenesulfonamide; sodium azide; manganese (II) chloride; E317A-mutant of bovine α3-galactosyltransferase in various solvent(s) T=30°C; pH=7.0; Enzyme kinetics; Further Variations:Catalysts;
参考文献
Journal of the American Chemical Society, , vol. 128, # 50 p. 16030 - 16031
反应条件
N-chloro-succinimide; lithium azide; triphenylphosphine in N,N-dimethyl-formamide T=5°C; 96 h; Yield given. Yields of byproduct given;
参考文献
Tetrahedron Letters, , vol. 35, # 14 p. 2175 - 2178
反应条件
1: sodium azide; tetra(n-butyl)ammonium hydrogensulfate; potassium carbonate / dichloromethane; water / 20 °C / Inert atmosphere 2: methanol; sodium methylate / 20 °C / Inert atmosphere View Scheme
参考文献
Chemical Communications, , vol. 48, # 4 p. 522 - 524
反应条件
1: sodium acetate / |Reflux 2: acetic acid; hydrogen bromide / dichloromethane / 0 - 25 °C 3: sodium azide / dimethyl sulfoxide / 0.5 h / 25 °C 4: sodium methylate / methanol / 24 h / 25 °C / pH 9 - 10 View Scheme
参考文献
Journal of the American Chemical Society, , vol. 135, # 24 p. 9055 - 9077
反应条件
hydrogen; platinum(IV) oxide in methanol
参考文献
Tamura, Masahiro; Nishizaki, Hiroshi; Miyazaki, Chiemi; Okai, Hideo
Bulletin of the Chemical Society of Japan, 1984 , vol. 57, # 11 p. 3167 - 3172
参考文献
Monegal, Ana; Planas, Antoni
Journal of the American Chemical Society, 2006 , vol. 128, # 50 p. 16030 - 16031
反应条件
triphenylphosphine
24 h; Ambient temperature;
参考文献
Kovacs, Jozsef; Pinter, Istvan; Messmer, Andras; Toth, Gabor
Carbohydrate Research, 1985 , vol. 141, p. 57 - 66
