3',5'-二-O-苯甲酰基胸苷合成路线 （共 13 条）
反应条件
9-ethyl-3,6-dimethoxy-9H-carbazole; isopropyl alcohol in water T=45°C; P=1034.32 Torr; 0.166667 h; UV-irradiation; Reagent/catalystTemperatureSolvent;
参考文献
Shen, Bo; Jamison, Timothy F.
Australian Journal of Chemistry, 2013 , vol. 66, # 2 p. 157 - 164
反应条件
4-(N,N-dimethlyamino)pyridine in various solvent(s) T=50°C; 2 h;
参考文献
Kumar, Vineet; Parmar, Virinder S.; Malhotra, Sanjay V.
Tetrahedron Letters, 2007 , vol. 48, # 5 p. 809 - 812
反应条件
pyridine; 4-(N,N-dimethlyamino)pyridine T=40°C; 5 h;
参考文献
Prasad, Ashok K.; Kumar, Vineet; Maity, Jyotirmoy; Wang, Zhiwei; Ravikumar, Vasulinga T.; Sanghvi, Yogesh S.; Parmar, Virinder S.
Synthetic Communications, 2005 , vol. 35, # 7 p. 935 - 945
反应条件
pyridine T=50 - 55°C; 72 h;
参考文献
Li; Sun; Ogura; Konda; Sasaki; Toda; Takayanagi; Harigaya
Chemical and Pharmaceutical Bulletin, 1995 , vol. 43, # 1 p. 144 - 146
反应条件
anhydrous magnesium perchlorate; 9-ethyl-3,6-dimethylcarbazole in water; isopropyl alcohol Elimination; deoxygenation; 1.5 h; Photolysis;
参考文献
Journal of Organic Chemistry, , vol. 65, # 19 p. 5969 - 5985
反应条件
anhydrous magnesium perchlorate; 9-ethyl-3,6-dimethylcarbazole in water; isopropyl alcohol T=0°C; Elimination; deoxygenation; Photolysis;
参考文献
Journal of Organic Chemistry, , vol. 65, # 19 p. 5969 - 5985
反应条件
1: 98 percent / SnCl4 / acetonitrile / 20 °C 2: 52 percent / 3,6-dimethyl-9-ethylcarbazole; Mg(ClO4)2 / propan-2-ol; H2O / 1.5 h / Photolysis View Scheme
参考文献
Journal of Organic Chemistry, , vol. 65, # 19 p. 5969 - 5985
反应条件
1: 97 percent / 2,6-lutidine / CH2Cl2 / 2.5 h / 20 °C 2: 98 percent / SnCl4 / acetonitrile / 20 °C 3: 52 percent / 3,6-dimethyl-9-ethylcarbazole; Mg(ClO4)2 / propan-2-ol; H2O / 1.5 h / Photolysis View Scheme
参考文献
Journal of Organic Chemistry, , vol. 65, # 19 p. 5969 - 5985
反应条件
2: 3,6-dimethyl-9-ethylcarbazole; Mg(ClO4)2 / propan-2-ol; H2O / 0 °C / Photolysis View Scheme
参考文献
Journal of Organic Chemistry, , vol. 65, # 19 p. 5969 - 5985
反应条件
1: 2,6-di-tert-butyl-4-methylpyridinium triflate / acetonitrile / 0.5 h / 150 °C / 5171.62 Torr 2: 9-ethyl-3,6-dimethoxy-9H-carbazole; isopropyl alcohol / water / 0.17 h / 45 °C / 1034.32 Torr / |UV-irradiation View Scheme
参考文献
Australian Journal of Chemistry, , vol. 66, # 2 p. 157 - 164
