(Z)-8-十四碳烯-1-醇乙酸酯合成路线 (共 8 条)
反应条件
in pyridine 24 h; Ambient temperature;
参考文献
Odinokov, V. N.; Akhmetova, V. R.; Khasanov, Kh. D.; Abduvakhabov, A. A.; Tolstikov, G. A.; Panasenko, A. A.
Chemistry of Natural Compounds, 1989 , vol. 25, p. 240 - 243
Khimiya Prirodnykh Soedinenii, 1989 , # 2 p. 276 - 279
反应条件
1: 94.7 percent / acetonitrile 2: 68 percent / DMSO, NaH / tetrahydrofuran / 0.5 h 3: pyridine View Scheme
参考文献
Horiike; Tanouchi; Hirano
Agricultural and Biological Chemistry, 1980 , vol. 44, # 2 p. 257 - 261
反应条件
1: 68 percent / DMSO, NaH / tetrahydrofuran / 0.5 h 2: pyridine View Scheme
参考文献
Horiike; Tanouchi; Hirano
Agricultural and Biological Chemistry, 1980 , vol. 44, # 2 p. 257 - 261
反应条件
1: 68 percent / DMSO, NaH / tetrahydrofuran / 0.5 h 2: pyridine View Scheme
参考文献
Horiike; Tanouchi; Hirano
Agricultural and Biological Chemistry, 1980 , vol. 44, # 2 p. 257 - 261
反应条件
1: 80 percent / 1.) ozone, NaHCO3, 2.) triethylamine / 1.) CH2Cl2, MeOH, -70 deg C, 2.) -20 deg C, 3h, 3.) 8 deg C, 15h 2: tert-BuOK 3: 90 percent / (iso-C4H9)2AlH / toluene; diethyl ether / 1.) 0 deg C, 2h, 2.) room temperature, 15h 4: 74 percent / pyridine / 24 h / Ambient temperature View Scheme
参考文献
Odinokov, V. N.; Akhmetova, V. R.; Khasanov, Kh. D.; Abduvakhabov, A. A.; Tolstikov, G. A.; Panasenko, A. A.
Chemistry of Natural Compounds, 1989 , vol. 25, p. 240 - 243
Khimiya Prirodnykh Soedinenii, 1989 , # 2 p. 276 - 279
反应条件
1: tert-BuOK 2: 90 percent / (iso-C4H9)2AlH / toluene; diethyl ether / 1.) 0 deg C, 2h, 2.) room temperature, 15h 3: 74 percent / pyridine / 24 h / Ambient temperature View Scheme
参考文献
Odinokov, V. N.; Akhmetova, V. R.; Khasanov, Kh. D.; Abduvakhabov, A. A.; Tolstikov, G. A.; Panasenko, A. A.
Chemistry of Natural Compounds, 1989 , vol. 25, p. 240 - 243
Khimiya Prirodnykh Soedinenii, 1989 , # 2 p. 276 - 279
反应条件
1: 90 percent / (iso-C4H9)2AlH / toluene; diethyl ether / 1.) 0 deg C, 2h, 2.) room temperature, 15h 2: 74 percent / pyridine / 24 h / Ambient temperature View Scheme
参考文献
Odinokov, V. N.; Akhmetova, V. R.; Khasanov, Kh. D.; Abduvakhabov, A. A.; Tolstikov, G. A.; Panasenko, A. A.
Chemistry of Natural Compounds, 1989 , vol. 25, p. 240 - 243
Khimiya Prirodnykh Soedinenii, 1989 , # 2 p. 276 - 279
反应条件
pyridine Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Horiike; Tanouchi; Hirano
Agricultural and Biological Chemistry, 1980 , vol. 44, # 2 p. 257 - 261