磷酸三（2,2,2-三氟乙基）酯合成路线 （共 20 条）
反应条件
phosphorus pentachloride T=20°C; 12 h;
参考文献
Timperley, Christopher M.; Holden, Ian; Morton, Ian J.; Waters, Matthew J.
Journal of Fluorine Chemistry, 2000 , vol. 106, # 2 p. 153 - 161
参考文献
Lowther, Nicholas; Crook, Polly; Hall, C. Dennis
Phosphorus, Sulfur and Silicon and the Related Elements, 1995 , vol. 102, # 1-4 p. 195 - 204
反应条件
triethylamine in diethyl ether T=20°C; Esterification; 12 h;
参考文献
Timperley, Christopher M.; Bird, Michael; Broderick, John F.; Holden, Ian; Morton, Ian J.; Waters, Matthew J.
Journal of Fluorine Chemistry, 2000 , vol. 104, # 2 p. 215 - 223
反应条件
trichlorophosphate; calcium chloride 3.5 h; Heating;
参考文献
Goryunov, E. I.; Petrovskii, P. V.; Shcherbina, T. M.; Laretina, A. P.; Zakharov, L. S.; Kabachnik, M. I.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1990 , vol. 39, # 4.2 p. 787 - 794
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1990 , # 4 p. 878 - 886
反应条件
4-(N,N-dimethlyamino)pyridine; 3-hydroxy-1-propanethiol; triethylamine in diethyl ether T=0 - 20°C; 12 h; Title compound not separated from byproducts;
参考文献
Timperley, Christopher M.; Saunders, Sally A.; Szpalek, Josef; Waters, Matthew J.
Journal of Fluorine Chemistry, 2003 , vol. 119, # 2 p. 161 - 171
反应条件
4-(N,N-dimethlyamino)pyridine; ethane-1,2-dithiol; triethylamine in diethyl ether T=0 - 20°C; 12 h; Title compound not separated from byproducts;
参考文献
Timperley, Christopher M.; Saunders, Sally A.; Szpalek, Josef; Waters, Matthew J.
Journal of Fluorine Chemistry, 2003 , vol. 119, # 2 p. 161 - 171
反应条件
bromine; triethylamine in diethyl ether 1.) -50 deg to -60 deg C, 1.5 h, 2.) 20 deg C, 12 h;
参考文献
Mironov; Bredikhin; Bredikhina; Novikova; Konovalova
Russian Journal of General Chemistry, 1997 , vol. 67, # 8 p. 1204 - 1207
反应条件
cyclohexane-1,2-epoxide in neat (no solvent) T=34°C; 4.16667 h; UV-irradiation;
参考文献
Nalli, Thomas W.; Stanek, Lee G.; Molenaar, Rebekka H.; Weidell, Krysia L.; Meyer, Justin P.; Johnson, Brandon R.; Steckler, Timothy T.; Wackerly, Jay Wm.; Studler, Missy Jo; Vickerman, Kevin L.; Klankowski, Stephen A.
Journal of Organic Chemistry, 2013 , vol. 78, # 8 p. 3561 - 3569
反应条件
cyclohexane-1,2-epoxide in acetonitrile-D3 T=34°C; 4.5 h; UV-irradiation;
参考文献
Nalli, Thomas W.; Stanek, Lee G.; Molenaar, Rebekka H.; Weidell, Krysia L.; Meyer, Justin P.; Johnson, Brandon R.; Steckler, Timothy T.; Wackerly, Jay Wm.; Studler, Missy Jo; Vickerman, Kevin L.; Klankowski, Stephen A.
Journal of Organic Chemistry, 2013 , vol. 78, # 8 p. 3561 - 3569
反应条件
sodium hydroxide in chloroform 3 h;
参考文献
Timperley, Christopher M.; Marriott, Stephen N.; Waters, Matthew J.
Journal of Fluorine Chemistry, 2002 , vol. 113, # 1 p. 111 - 122
