Alpha-(三氟甲基)乙烯硼酸合成路线 （共 4 条）
反应条件
magnesium in tetrahydrofuran T=0°C; 4 h;
参考文献
Billen, Denis; Chubb, Nathan Anthony Logan; Gethin, David Morris; Hall, Kim Thomas; Roberts, Lee Richard; Walshe, Nigel Derek Arthur
Patent: US2005/148649 A1, 2005 ;
Location in patent: Page/Page column 27 ;
反应条件
boric acid trimethyl ester; magnesium in tetrahydrofuran T=20°C; 4 h;
参考文献
Jiang, Biao; Wang, Quan-Fu; Yang, Cai-Guang; Xu, Min
Tetrahedron Letters, 2001 , vol. 42, # 24 p. 4083 - 4085
反应条件
tetrakis(triphenylphosphine) palladium(0); sodium carbonate in methanol; toluene T=70°C; Suzuki cross-coupling; 6 h;
参考文献
Jiang, Biao; Wang, Quan-Fu; Yang, Cai-Guang; Xu, Min
Tetrahedron Letters, 2001 , vol. 42, # 24 p. 4083 - 4085
反应条件
tetrakis(triphenylphosphine) palladium(0); sodium carbonate in methanol; water; toluene T=70°C; Suzuki-Miyaura coupling; 32 h; Inert atmosphere;
参考文献
Ichikawa, Junji; Ikeda, Masahiro; Hattori, Masahiro
Heterocycles, 2009 , vol. 77, # 2 p. 1285 - 1296
