萘并[2,3-c]吖啶-5,8,14(13H)-三酮合成路线 （共 21 条）
参考文献
Ullmann; Dootson
Chemische Berichte, 1918 , vol. 51, p. 14
反应条件
1: 1) NaNO2/H2SO4; 2) NaN3 / 1) AcOH, 20-25 deg C, 15-20 min; 2) H2O, 10-15 min 2: nitrobenzene / 7 h / Heating View Scheme
参考文献
Gornostaev, L. M.; Levdanskii, V. A.; Arnol'd, E. V.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1983 , p. 19 - 21
Khimiya Geterotsiklicheskikh Soedinenii, 1983 , vol. 19, # 1 p. 22 - 25
反应条件
1: potassium carbonate; copper oxide; nitrobenzene 2: sulfuric acid / 120 - 130 °C View Scheme
参考文献
Ullmann; Dootson
Chemische Berichte, 1918 , vol. 51, p. 14
参考文献
Bayer and Co.
Patent: DE262469 ;
Fortschr. Teerfarbenfabr. Verw. Industriezweige, vol. 11, p. 687
Full Text Show Details
Ullmann; Bincer
Chemische Berichte, 1916 , vol. 49, p. 740
反应条件
in nitrobenzene 7 h; Heating; Yield given;
参考文献
Gornostaev, L. M.; Levdanskii, V. A.; Arnol'd, E. V.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1983 , p. 19 - 21
Khimiya Geterotsiklicheskikh Soedinenii, 1983 , vol. 19, # 1 p. 22 - 25
反应条件
1: potassium acetate; copper acetate; copper powder / 150 - 160 °C / weiteres Reagens: Isoamylalkohol 2: concentrated sulfuric acid / 100 - 110 °C View Scheme
参考文献
Ullmann; Ochsner
Justus Liebigs Annalen der Chemie, 1911 , vol. 381, p. 8
Full Text Show Details
Ullmann
Chemische Berichte, 1910 , vol. 43, p. 537
Chem. Zentralbl., 1910 , vol. 81, # II p. 1422
反应条件
sodium acetate; nitrobenzene; copper dichloride
参考文献
Bayer and Co.
Patent: DE285771 ;
Fortschr. Teerfarbenfabr. Verw. Industriezweige, vol. 12, p. 257
Full Text Show Details
Bayer and Co.
Patent: DE236407 ;
Fortschr. Teerfarbenfabr. Verw. Industriezweige, vol. 10, p. 632
反应条件
in nitrobenzene 7 h; Heating; Yield given;
参考文献
Gornostaev, L. M.; Levdanskii, V. A.; Arnol'd, E. V.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1983 , p. 19 - 21
Khimiya Geterotsiklicheskikh Soedinenii, 1983 , vol. 19, # 1 p. 22 - 25
反应条件
1: potassium carbonate; copper oxide; nitrobenzene 2: sulfuric acid / 120 - 130 °C View Scheme
参考文献
Schaarschmidt
Justus Liebigs Annalen der Chemie, 1914 , vol. 405, p. 120
Chem. Zentralbl., 1914 , vol. 85, # I p. 720
反应条件
1: potassium acetate; copper acetate; copper powder / 150 - 160 °C / weiteres Reagens: Isoamylalkohol 2: concentrated sulfuric acid / 100 - 110 °C View Scheme
参考文献
Ullmann
Chemische Berichte, 1910 , vol. 43, p. 537
Chem. Zentralbl., 1910 , vol. 81, # II p. 1422
