5,5,6,6,7,7,7-七氟庚烷-2,4-二酮合成路线 （共 6 条）
反应条件
1: ethyl 2,2,3,3,4,4,4-heptafluorobutyrate With sodium methylate in methanol; diethyl ether T=0°C; 0.5 h; 2: acetone in methanol; diethyl ether T=20°C; Claisen condensation; 16 h; Further stages.;
参考文献
Buettner, Stefan; Lubbe, Mathias; Reinke, Helmut; Fischer, Christine; Langer, Peter
Tetrahedron, 2008 , vol. 64, # 34 p. 7968 - 7976
反应条件
sodium hydride in diethyl ether
参考文献
Peglion, Jean-Louis; Pastor, Raphael-Emile; Cambon, Aime-Roger
Bulletin de la Societe Chimique de France, 1980 , vol. 2, # 5-6 p. 309 - 315
反应条件
hydrogenchloride 1 h; Heating;
参考文献
Kurykin; Vol'pin; German
Journal of Fluorine Chemistry, 1996 , vol. 80, # 1 p. 9 - 12
反应条件
1: 88 percent / NH3 / diethyl ether / 1 h / Ambient temperature 2: 76 percent / aq. HCl / 1 h / Heating View Scheme
参考文献
Journal of Fluorine Chemistry, , vol. 80, # 1 p. 9 - 12
反应条件
water Heatingother reagent; Product distribution;
参考文献
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), , vol. 36, # 9 p. 1962 - 1964
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, , # 9 p. 2112 - 2113
反应条件
hydrogenchloride; hydrazine in methanol T=60°C; 3 h; Heating;
参考文献
Peglion, Jean-Louis; Pastor, Raphael-Emile; Cambon, Aime-Roger
Bulletin de la Societe Chimique de France, 1980 , vol. 2, # 5-6 p. 309 - 315
