反应条件
1: 1-(tetrahydropyran-2-yloxy)-4-pentyne With n-butyllithium in tetrahydrofuran; hexane T=0°C; 0.25 h; 2: With N,N,N',N',N'',N''-hexamethylphosphoric triamide in tetrahydrofuran; hexane T=0°C; 0.25 h; 3: tridecyl iodide in tetrahydrofuran; N,N,N',N',N'',N''-hexamethylphosphoric triamide; hexane 20 h;
参考文献
Fletcher, Steven; Ahmad, Ayesha; Perouzel, Eric; Jorgensen, Michael R.; Miller, Andrew D.
Organic and Biomolecular Chemistry, 2006 , vol. 4, # 2 p. 196 - 199
