4-硝基苯基-BETA-D-吡喃甘露糖苷合成路线 （共 14 条）
反应条件
sodium methylate in methanol T=4°C;
参考文献
Baggett, Neil; Marsden, Brian J.
Carbohydrate Research, 1983 , vol. 119, p. 285 - 291
反应条件
Dowex-1 (basic) resin in methanol Ambient temperature;
参考文献
Kleine, Henry P.; Sidhu, Ravinder S.
Carbohydrate Research, 1988 , vol. 182, p. 307 - 312
反应条件
1: 74 percent / dicyclohexyl-18-crown-6 / acetonitrile / Ambient temperature 2: 47 percent / Dowex-1 (basic) resin / methanol / Ambient temperature View Scheme
参考文献
Carbohydrate Research, , vol. 182, p. 307 - 312
反应条件
1: 74 percent / dicyclohexyl-18-crown-6 / acetonitrile / Ambient temperature 2: 47 percent / Dowex-1 (basic) resin / methanol / Ambient temperature View Scheme
参考文献
Carbohydrate Research, , vol. 182, p. 307 - 312
反应条件
1: boron trifluoride diethyl etherate / dichloromethane / 0 - 20 °C / |Inert atmosphere 2: methanol; sodium methylate / 20 °C / pH 10 - 11 View Scheme
参考文献
European Journal of Organic Chemistry, , # 12 p. 2414 - 2419
反应条件
1: boron trifluoride diethyl etherate / dichloromethane / 0 - 20 °C / |Inert atmosphere 2: methanol; sodium methylate / 20 °C / pH 10 - 11 View Scheme
参考文献
European Journal of Organic Chemistry, , # 12 p. 2414 - 2419
反应条件
1: 1.) phosphorus(V)oxide; 2.) sodium borohydride; 3.) pyridine / 1.) dimethyl sulfoxide, N,N-dimethylformamide, 2 h, 45-50 deg C; 2.) methanol, 30 min, r.t.; 3.) 16 h r.t. 2: 73 percent / sodium methoxide / methanol / 4 °C View Scheme
参考文献
Carbohydrate Research, , vol. 119, p. 285 - 291
反应条件
1: 62 percent / silver(I)carbonate, calcium sulphate / acetone / 3 h / Ambient temperature 2: 1.) phosphorus(V)oxide; 2.) sodium borohydride; 3.) pyridine / 1.) dimethyl sulfoxide, N,N-dimethylformamide, 2 h, 45-50 deg C; 2.) methanol, 30 min, r.t.; 3.) 16 h r.t. 3: 73 percent / sodium methoxide / methanol / 4 °C View Scheme
参考文献
Carbohydrate Research, , vol. 119, p. 285 - 291
反应条件
1: 62 percent / silver(I)carbonate, calcium sulphate / acetone / 3 h / Ambient temperature 2: 1.) phosphorus(V)oxide; 2.) sodium borohydride; 3.) pyridine / 1.) dimethyl sulfoxide, N,N-dimethylformamide, 2 h, 45-50 deg C; 2.) methanol, 30 min, r.t.; 3.) 16 h r.t. 3: 73 percent / sodium methoxide / methanol / 4 °C View Scheme
参考文献
Carbohydrate Research, , vol. 119, p. 285 - 291
反应条件
1: EtO2CN=NCO2Et, Ph3P / toluene / Ambient temperature 2: 90percent aq. CF3CO2H / 1 h View Scheme
参考文献
Chemical & Pharmaceutical Bulletin, , vol. 31, # 11 p. 3902 - 3905
