2,6-二苯基吡喃高氯酸盐合成路线 （共 16 条）
反应条件
in N,N-dimethyl-formamide 1 h; Heating;
参考文献
Zhdanov, Yu. A.; Zvezdina, E. A.; Statsenko, S. M.; Maksimova, A. N.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1987 , vol. 23, # 2 p. 149 - 154
Khimiya Geterotsiklicheskikh Soedinenii, 1987 , vol. 23, # 2 p. 182 - 187
参考文献
Zhdanov, Yu. A.; Zvezdina, E. A.; Statsenko, S. M.; Maksimova, A. N.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1987 , vol. 23, # 2 p. 149 - 154
Khimiya Geterotsiklicheskikh Soedinenii, 1987 , vol. 23, # 2 p. 182 - 187
参考文献
Zhdanov, Yu. A.; Zvezdina, E. A.; Statsenko, S. M.; Maksimova, A. N.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1987 , vol. 23, # 2 p. 149 - 154
Khimiya Geterotsiklicheskikh Soedinenii, 1987 , vol. 23, # 2 p. 182 - 187
反应条件
N,N-dicyclohexylethylamine in acetonitrile 3 h;
参考文献
Reynolds, G. A.; Chen, C. H.
Journal of Heterocyclic Chemistry, 1981 , vol. 18, p. 1235 - 1237
反应条件
in N,N-dimethyl-formamide T=150°C; 3 h; Inert atmosphere;
参考文献
Abalos, Tatiana; Royo, Santiago; Martinez-Manez, Ramon; Sancenon, Felix; Soto, Juan; Costero, Ana M.; Gil, Salvador; Parra, Margarita
New Journal of Chemistry, 2009 , vol. 33, # 8 p. 1641 - 1645
反应条件
sodium ethanolate in ethanol; acetone 1 h; Heating;
参考文献
Zvezdina, E. A.; Zhdanova, M. P.; Giryavenko, I. I.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1983 , vol. 19, # 7 p. 714 - 719
Khimiya Geterotsiklicheskikh Soedinenii, 1983 , vol. 19, # 7 p. 893 - 898
反应条件
(i) Et2O, (ii) aq. HCl; Multistep reaction;
参考文献
Dimroth,K. et al.
Justus Liebigs Annalen der Chemie, 1964 , vol. 678, p. 183 - 201
反应条件
1: 1.) n-butyllithium / 1.) ether, hexane, -77 deg C, 15 min; 2.) ether, room temp., 1 h
2: 1.) n-butyllithium / 1.) THF, hexane, <-5 deg C, 5 min; 2.) THF, room temp., 1 h
View Scheme
参考文献
Doney, Jeffrey J.; Chen, Chin H.
Synthesis, 1983 , # 6 p. 491 - 492
反应条件
1: 1.) n-butyllithium / 1.) ether, hexane, -77 deg C, 15 min; 2.) ether, room temp., 1 h
2: 1.) n-butyllithium / 1.) THF, hexane, <-5 deg C, 5 min; 2.) THF, room temp., 1 h
View Scheme
参考文献
Doney, Jeffrey J.; Chen, Chin H.
Synthesis, 1983 , # 6 p. 491 - 492
反应条件
1: 1.) n-butyllithium / 1.) ether, hexane, -77 deg C, 15 min; 2.) ether, room temp., 1 h
2: 1.) n-butyllithium / 1.) THF, hexane, <-5 deg C, 5 min; 2.) THF, room temp., 1 h
View Scheme
参考文献
Doney, Jeffrey J.; Chen, Chin H.
Synthesis, 1983 , # 6 p. 491 - 492
