1: With isopropylmagnesium chloride in tetrahydrofuran T=-20 - 0°C; 0.5 h; 2: With boric acid trimethyl ester in tetrahydrofuran T=20°C; 1 h; 3: With peracetic acid in tetrahydrofuran T=-20 - 20°C; 0.5 h;
参考文献
Balko, Terry W.; Schmitzer, Paul R.; Daeuble, John F.; Yerkes, Carla N.; Siddall, Thomas L.
Patent: US2007/179060 A1, 2007 ;
Location in patent: Page/Page column 14 ;