1H,1H,2H-七氟-1-戊烯合成路线 (共 8 条)
反应条件
phosphorus pentoxide
参考文献
Pierce et al.
Journal of the American Chemical Society, 1953 , vol. 75, p. 5618
反应条件
1: NaOH / diethyl ether 2: Irradiation View Scheme
参考文献
Atherton,J.H. et al.
Journal of the Chemical Society [Section] C: Organic, 1971 , p. 366 - 371
反应条件
AlF2.8Cl0.2 1.) 25 deg C, 2 h, 2.) 60 deg C, 4 h;
参考文献
Krespan, Carl G.; Dixon, David A.
Journal of Fluorine Chemistry, 1996 , vol. 77, # 2 p. 117 - 126
参考文献
Atherton,J.H. et al.
Journal of the Chemical Society [Section] C: Organic, 1971 , p. 366 - 371
反应条件
calcium sulfate; hydrogen bromide; carbon T=120 - 140°C;
参考文献
Pierce et al.
Journal of the American Chemical Society, 1953 , vol. 75, p. 5618
反应条件
1: 66 percent / chlorine / neat (no solvent) / Irradiation
2: 1.) zinc; 2.) HCl / 1.) DMF, 100 deg C, 1 h
View Scheme
参考文献
Burton, Donald J.; Spawn, Terence D.
Journal of Fluorine Chemistry, 1988 , vol. 38, p. 119 - 124
反应条件
trichlorosilane
Irradiation.mit γ-Strahlen;
参考文献
El-Abbady; Anderson
Journal of the American Chemical Society, 1958 , vol. 80, p. 1737
反应条件
bromine; carbon
T=114 - 143°C;
参考文献
Pierce et al.
Journal of the American Chemical Society, 1953 , vol. 75, p. 5618