6-溴-3-甲基-1,3-苯并噻唑-2(3h)-酮合成路线 （共 6 条）
反应条件
potassium carbonate in dimethyl sulfoxide T=20°C;
参考文献
NOVARTIS AG; ADAMS, Christopher Michael; CHAMOIN, Sylvie; HU, Qi-Ying; ZHANG, Chun
Patent: WO2010/130794 A1, 2010 ;
Location in patent: Page/Page column 110 ;
WO 2010/130794 A1
反应条件
K2S; copper(ll) bromide T=120°C; 15 h;
参考文献
Yang, Yuan; Zhang, Xiaoyun; Zeng, Weilan; Huang, Hui; Liang, Yun
RSC Advances, 2014 , vol. 4, # 12 p. 6090 - 6093
反应条件
1: 81 percent / K2CO3 / butan-2-one / Heating 2: 16 percent Chromat. / 48percent HBr, PhOH / 5.5 h / Heating View Scheme
参考文献
Mellor, Michael; Osbourn, Susan E.
Tetrahedron, 1991 , vol. 47, # 12-13 p. 2255 - 2262
反应条件
bromine in chloroform
参考文献
Carato; Moussavi; Yous; Poupaert; Lebegue; Berthelot
Synthetic Communications, 2004 , vol. 34, # 14 p. 2601 - 2609
反应条件
hydrogen bromide; phenol 5.5 h; Heating;
参考文献
Mellor, Michael; Osbourn, Susan E.
Tetrahedron, 1991 , vol. 47, # 12-13 p. 2255 - 2262
反应条件
hydrogen bromide 6 h; Heatingalso in the presence of phenol; Mechanism;
参考文献
Mellor, Michael; Osbourn, Susan E.
Tetrahedron, 1991 , vol. 47, # 12-13 p. 2255 - 2262
