1-氯-1,1,2,2-四氟乙烷合成路线 (共 58 条)
反应条件
fluorine in various solvent(s) T=-75°C; 8 h;
参考文献
Conte, L.; Gambaretto, G. P.; Napoli, M.; Gervasutti, C.
Journal of Fluorine Chemistry, 1988 , vol. 38, p. 319 - 326
反应条件
tetrakis(triphenylphosphine) palladium(0) in hexane T=60°C; 0.5 h;
参考文献
Huang, Yao-Zeng; Shou, Qi-Lin
Journal of Organic Chemistry, 1987 , vol. 52, # 16 p. 3552 - 3558
反应条件
sulfur(IV) fluoride; lead dioxide T=100°C; 2 h;
参考文献
Bissell,E.R.; Fields,D.B.
Journal of Organic Chemistry, 1964 , vol. 29, p. 1591 - 1593
反应条件
Ni(PPh3)4 in 1,4-dioxane T=80°C; 6 h;
参考文献
Zhou, Qi-Lin; Huang, Yao-Zeng
Journal of Fluorine Chemistry, 1988 , vol. 39, p. 87 - 98
反应条件
hydrogenchloride; carbon T=300°C;
参考文献
Kinetic Chem. Inc.
Patent: US2365516 , 1940 ;
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Kinetic Chem. Inc.
Patent: US2393304 , 1940 ;
Full Text Show Details
Kinetic Chem. Inc.
Patent: US2343252 , 1940 ;
反应条件
an activated AlF3 T=210 - 240°C; 0.00972222 h; Gas phasea fluid-bed reactor; Product distribution / selectivity;
参考文献
Solvay Solexis S.p.A.
Patent: EP1502906 A1, 2005 ;
Location in patent: Page 7-8 ;
反应条件
palladium on activated charcoal T=120°C; Hydrogenation;
参考文献
Bitner et al.
U.S.Dep.Comm.Tech.Serv.Rep., 1958 , vol. 136732, p. 25
反应条件
triethylsilane; meta-chloroperoxybenzoic acid; 1,1,1,2-tetrafluorodichloroethane 1) 25 deg C, 1 h, 2) 100 deg C, 4 h; Yield givenYields of byproduct given;
参考文献
Petrov, Viacheslav A.
Journal of Organic Chemistry, 1998 , vol. 63, # 21 p. 7294 - 7297
参考文献
Park et al.
Industrial and Engineering Chemistry, 1947 , vol. 39, p. 357
Full Text Show Details
Kinetic Chem. Inc.
Patent: US2384449 , 1943 ;
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Kinetic Chem. Inc.
Patent: US2384821 , 1943 ;
反应条件
T=550 - 784°C; Various reactorsPyrolysis; Product distribution / selectivity;
参考文献
Noelke, Charles Joseph; Rao, Velliyur Nott Mallikarjuna
Patent: US2005/137430 A1, 2005 ;
Location in patent: Page/Page column 4 ;