1-氯-1,1,2,2-四氟乙烷合成路线 （共 58 条）
反应条件
chlorine 1 h; Gas phasePhotolysis;
参考文献
E.I. DUPONT DE NEMOURS AND COMPANY
Patent: WO2006/69108 A1, 2006 ;
Location in patent: Page/Page column 12 ;
反应条件
hydrogen fluoride; cobalt-substituted chromium oxide (Cr/Co 90/10, 12-20 mesh, (1.68 to 0.84 mm) ), prepared from chromium (III) nitrate, cobalt (II) nitrate, ammonia, ammonia nitrate (400°C) T=200 - 425°C; 9.33333 h;
参考文献
E.I. DU PONT DE NEMOURS AND COMPANY; Nappa, Mario, J.
Patent: WO2004/18396 A1, 2004 ;
Location in patent: Page 17-18 ;
反应条件
hydrogen fluoride; cobalt-substituted chromium oxide (Cr/Co 90/10, 12-20 mesh, (1.68 to 0.84 mm) ), prepared from chromium (III) nitrate, cobalt (II) nitrate, ammonia (400°C) T=200 - 425°C; 9.33333 h;
参考文献
E.I. DU PONT DE NEMOURS AND COMPANY; Nappa, Mario, J.
Patent: WO2004/18396 A1, 2004 ;
Location in patent: Page 13-14 ;
反应条件
hydrogen fluoride; Catalyst M-Chromium oxide T=200 - 425°C; 9.33333 h;
参考文献
E.I. DU PONT DE NEMOURS AND COMPANY; Nappa, Mario, J.
Patent: WO2004/18396 A1, 2004 ;
Location in patent: Page 19-20 ;
反应条件
hydrogen fluoride; cobalt-substituted chromium oxide (Cr/Co 95/5, 12-20 mesh, (1.68 to 0.84 mm) ), prepared from chromium (III) nitrate, cobalt (II) nitrate, ammonia, ammonia nitrate (400°C) T=200 - 425°C; 9.33333 h;
参考文献
E.I. DU PONT DE NEMOURS AND COMPANY; Nappa, Mario, J.
Patent: WO2004/18396 A1, 2004 ;
Location in patent: Page 16-17 ;
反应条件
hydrogen fluoride; antimony(V) pentachloride T=125°C;
参考文献
Henne
Journal of the American Chemical Society, 1938 , vol. 60, p. 1570
反应条件
hydrogen fluoride; mercury(II) oxide T=20°C;
参考文献
Henne
Journal of the American Chemical Society, 1938 , vol. 60, p. 1570
反应条件
fluorine T=-90°C; 1.5 h;
参考文献
Solvay Solexis S.p.A.
Patent: EP1388531 A1, 2004 ;
Location in patent: Page column 9 ;
反应条件
fluorine T=-90°C; 1.5 h;
参考文献
Solvay Solexis S.p.A.
Patent: US2004/30146 A1, 2004 ;
Location in patent: Page 4-5 ;
反应条件
dimethylsulfide Irradiation;
参考文献
Zhang, Cheng-Pan; Chen, Qing-Yun; Xiao, Ji-Chang; Gu, Yu-Cheng
Journal of Fluorine Chemistry, 2009 , vol. 130, # 7 p. 671 - 673
