1-氟-1,1,2,2-四氯乙烷合成路线 (共 27 条)
反应条件
hydrogen fluoride; SbF3; SbF5 T=125 - 139°C; P=16351.6 - 18376.8 Torr; 3.7 h;
参考文献
RHODIA ORGANIQUE FINE LIMITED
Patent: WO2004/46071 A1, 2004 ;
Location in patent: Page column 9 ;
反应条件
fluoro chloride in 1,2,2-trifluoro-trichloroethane; ethyl acetate T=20 - 25°C; 0.5 h; Yields of byproduct given;
参考文献
Boguslavskaya, L. S.; Chuvatkin, N. N.; Panteleeva, I. Yu.
Journal of Organic Chemistry USSR (English Translation), 1982 , vol. 18, # 10 p. 1832 - 1842
Zhurnal Organicheskoi Khimii, 1982 , vol. 18, # 10 p. 2082 - 2094
反应条件
hydrogen fluoride T=225°C; P=25742.8 Torr;
参考文献
Barlow, M. G.; Coles, B.; Haszeldine, R. N.
Journal of Fluorine Chemistry, 1980 , vol. 15, p. 381 - 386
反应条件
fluoro chloride in 1,2,2-trifluoro-trichloroethane T=20 - 25°C; 30 h; Yield given;
参考文献
Boguslavskaya, L. S.; Chuvatkin, N. N.; Panteleeva, I. Yu.
Journal of Organic Chemistry USSR (English Translation), 1982 , vol. 18, # 10 p. 1832 - 1842
Zhurnal Organicheskoi Khimii, 1982 , vol. 18, # 10 p. 2082 - 2094
参考文献
Miller
Journal of the American Chemical Society, 1940 , vol. 62, p. 342
反应条件
hydrogen fluoride; oxygen; Ni/Cr catalyst T=310°C; P=5250.53 Torr; 0.00972222 h; Gas phase; Conversion of starting material;
参考文献
Arkema France
Patent: US2010/210884 A1, 2010 ;
Location in patent: Page/Page column 2-3 ;
反应条件
hydrogen fluoride; boron trifluoride T=140 - 160°C;
参考文献
Henne; Arnold
Journal of the American Chemical Society, 1948 , vol. 70, p. 759
反应条件
hydrogen fluoride; chlorine; antimony(V) pentachloride T=70°C; P=12751.3 Torr;
参考文献
Atofina
Patent: US6339178 B1, 2002 ;
Location in patent: Example 1 ;
参考文献
Kunshenko, B. V.; Mokhamed, Nagib Mukhtar; Omarov, V. O.; Muratov, N. N.; Yagupol'skii, L. M.
Journal of Organic Chemistry USSR (English Translation), 1992 , vol. 28, # 4.1 p. 511 - 518
Zhurnal Organicheskoi Khimii, 1992 , vol. 28, # 4 p. 672 - 680
反应条件
hydrogen fluoride; antimony(V) pentachloride T=107 - 118°C; unter Druck;
参考文献
Whalley
Journal of the Society of Chemical Industry, London, 1947 , vol. 66, p. 429