1-氧杂环十五烷-2-酮合成路线 (共 40 条)
反应条件
aluminum oxide; chlorine; 1,8-diazabicyclo[5.4.0]undec-7-ene 1.) irradiation, 20 deg C, 2 h, 2.) DMF, reflux, 8 h; Multistep reaction. Title compound not separated from byproducts;
参考文献
Hinkamp, Ludger; Schaefer, Hans J.; Wippich, Barbara; Luftmann, Heinrich
Liebigs Annalen der Chemie, 1992 , # 6 p. 559 - 564
反应条件
in xylene HeatingHamett study, primary isotope effect; Kinetics;
参考文献
Wollenberg, R. H.; Nimitz, J. S.; Gokcek, D. Y.
Tetrahedron Letters, 1980 , vol. 21, p. 2791 - 2794
反应条件
in xylene HeatingHammett study; Kinetics;
参考文献
Wollenberg, R. H.; Nimitz, J. S.; Gokcek, D. Y.
Tetrahedron Letters, 1980 , vol. 21, p. 2791 - 2794
反应条件
in xylene HeatingHammett study; Kinetics;
参考文献
Wollenberg, R. H.; Nimitz, J. S.; Gokcek, D. Y.
Tetrahedron Letters, 1980 , vol. 21, p. 2791 - 2794
反应条件
in xylene HeatingHammett study; Kinetics;
参考文献
Wollenberg, R. H.; Nimitz, J. S.; Gokcek, D. Y.
Tetrahedron Letters, 1980 , vol. 21, p. 2791 - 2794
反应条件
in xylene HeatingHammett study, primary isotopic effects; Kinetics;
参考文献
Wollenberg, R. H.; Nimitz, J. S.; Gokcek, D. Y.
Tetrahedron Letters, 1980 , vol. 21, p. 2791 - 2794
反应条件
in xylene HeatingHammett study; Kinetics;
参考文献
Wollenberg, R. H.; Nimitz, J. S.; Gokcek, D. Y.
Tetrahedron Letters, 1980 , vol. 21, p. 2791 - 2794
反应条件
in xylene HeatingHammett study; Kinetics;
参考文献
Wollenberg, R. H.; Nimitz, J. S.; Gokcek, D. Y.
Tetrahedron Letters, 1980 , vol. 21, p. 2791 - 2794
反应条件
hydrazine hydrate in ethanol Heating;
参考文献
Allen,C.F.H.; Weismann Magder,E.
Journal of Heterocyclic Chemistry, 1969 , vol. 6, p. 349 - 360
反应条件
hydrogen iodide in acetic acid
T=100°C;
参考文献
Kruizinga, Wim H.; Kellogg, Richard M.
Journal of the American Chemical Society, 1981 , vol. 103, # 17 p. 5183 - 5189