5-溴-苯并呋喃-2-甲酰胺合成路线 (共 6 条)
反应条件
ammonia in 1,4-dioxane; ethanol
参考文献
Lee, Jaekyoo; Khanapure, Subhash P.; Kim, Hwa-Ok; Rajur, Raj S. B.; Li, Bing; Williams, John D.; Pai, Ramdas; Peet, Norton P.
Synthetic Communications, 2010 , vol. 40, # 22 p. 3390 - 3396
反应条件
sodium t-butanolate; tris-(dibenzylideneacetone)dipalladium(0); tri-tert-butyl phosphine in diethylene glycol dimethyl ether T=20 - 120°C; 48 h;
参考文献
MERCK PATENT GMBH
Patent: WO2006/114202 A1, 2006 ;
Location in patent: Page/Page column 5-6 ;
反应条件
2,4,6-trichloro-1,3,5-triazine in N,N-dimethyl-formamide
参考文献
Lee, Jaekyoo; Khanapure, Subhash P.; Kim, Hwa-Ok; Rajur, Raj S. B.; Li, Bing; Williams, John D.; Pai, Ramdas; Peet, Norton P.
Synthetic Communications, 2010 , vol. 40, # 22 p. 3390 - 3396
反应条件
hydrogenchloride; Pd(dba)2 in diethylene glycol dimethyl ether; water
反应条件
hydrogenchloride; Pd(dba)2 in water; ethyl acetate; toluene
反应条件
hydrogenchloride; Pd(dba)2 in diethylene glycol dimethyl ether; water
参考文献
Bathe, Andreas; Emmert, Steffen; Helfert, Bernd; Boettcher, Henning
Patent: US2003/125558 A1, 2003 ;