暂无反应条件数据

暂无反应条件数据

1.1: HNO3; glacial AcOH / 1 h / 50 - 60 °C 2.1: Fe; aq. NH4Cl / methanol / 19 h / Heating 3.1: dimethylformamide / 2.3 h / Heating 4.1: n-BuLi / hexane; tetrahydrofuran / 0.33 h / -78 °C 4.2: hexane; tetrahydrofuran / 1 h / -78 °C 4.3: glacial acetic acid / tetrahydrofuran; hexane / -78 - 25 °C View Scheme

1.1: HNO3; glacial AcOH / 1 h / 50 - 60 °C 2.1: Fe; aq. NH4Cl / methanol / 19 h / Heating 3.1: dimethylformamide / 2.3 h / Heating 4.1: n-BuLi / hexane; tetrahydrofuran / 0.33 h / -78 °C 4.2: hexane; tetrahydrofuran / 1 h / -78 °C 4.3: glacial acetic acid / tetrahydrofuran; hexane / -78 - 25 °C 5.1: oxalyl chloride; DMF / CH2Cl2 / 48 h View Scheme