(R)-(-)-2-氨基-1-丙醇合成路线 (共 32 条)
反应条件
lithium aluminium tetrahydride in tetrahydrofuran 10 h; Heating; Yield given;
参考文献
Tetrahedron Letters, , vol. 28, # 19 p. 2083 - 2086
反应条件
hydrogen; 10percent Nishimura catalyst <(45.9percent Rh/19.9percent Pt) oxide> in methanol T=25°C; P=75007.5 Torr; 16 h;
参考文献
Advanced Synthesis and Catalysis, , vol. 343, # 8 p. 802 - 808
反应条件
hydrogen; 10percent Nishimura catalyst <(45.9percent Rh/19.9percent Pt) oxide> in methanol T=25°C; P=75007.5 Torr; 16 h;
参考文献
Advanced Synthesis and Catalysis, , vol. 343, # 8 p. 802 - 808
反应条件
hydrogen; 10percent Nishimura catalyst <(45.9percent Rh/19.9percent Pt) oxide> in methanol T=25°C; P=75007.5 Torr; 16 h;
参考文献
Advanced Synthesis and Catalysis, , vol. 343, # 8 p. 802 - 808
反应条件
hydrogen; platinum(IV) oxide in ethanol P=2482.3 Torr;
参考文献
Tetrahedron, , vol. 47, # 9 p. 1603 - 1610
反应条件
hydrogen; 10percent Nishimura catalyst <(45.9percent Rh/19.9percent Pt) oxide> in methanol T=25°C; P=75007.5 Torr; 16 h; Product distribution; Further Variations:Catalysts;
参考文献
Advanced Synthesis and Catalysis, , vol. 343, # 8 p. 802 - 808
反应条件
1: With titanium(IV) isopropylate; 1-dodecylamine; (-)-(R,R)-TADDOL in diphenylether T=90°C; 1 h; 2: Propylene glycol in diphenylether T=90°C; 0.166667 h; Product distribution / selectivity;
参考文献
US2009/30235 A1, ;
Page/Page column 14 ;
反应条件
chiral stationary phase including isopropyl-functionalized CF6 in methanol; acetic acid; triethylamine; acetonitrile T=20°C; Purification / work up;
参考文献
WO2010/148191 A2, ;
Page/Page column 45-49; 59 ;
参考文献
Science (Washington, DC, United States), , vol. 82, p. 17
Chem. Zentralbl., , vol. 106, # II p. 2821
反应条件
sodium tetrahydroborate in ethanol; water 5.5 h; Heating;
参考文献
Agricultural and Biological Chemistry, , vol. 51, # 2 p. 537 - 548